(S)-1-methyl-3-(2-((1-(ethyloxy)-1-oxo-3-phenylpropan-2-yl)amino)-2-oxoethyl)-1H-imidazol-3-ium bromide

Base Information

Chemical Name:(S)-1-methyl-3-(2-((1-(ethyloxy)-1-oxo-3-phenylpropan-2-yl)amino)-2-oxoethyl)-1H-imidazol-3-ium bromide
CAS No.:1379456-23-1
Molecular Formula:Br*C₁₇H₂₂N₃O₃
Molecular Weight:396.284
Hs Code.:

Synonyms:(S)-1-methyl-3-(2-((1-(ethyloxy)-1-oxo-3-phenylpropan-2-yl)amino)-2-oxoethyl)-1H-imidazol-3-ium bromide

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Chemical Property of (S)-1-methyl-3-(2-((1-(ethyloxy)-1-oxo-3-phenylpropan-2-yl)amino)-2-oxoethyl)-1H-imidazol-3-ium bromide

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Technology Process of (S)-1-methyl-3-(2-((1-(ethyloxy)-1-oxo-3-phenylpropan-2-yl)amino)-2-oxoethyl)-1H-imidazol-3-ium bromide

There total 3 articles about (S)-1-methyl-3-(2-((1-(ethyloxy)-1-oxo-3-phenylpropan-2-yl)amino)-2-oxoethyl)-1H-imidazol-3-ium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 616-47-7
1-methyl-1H-imidazole

: 32132-71-1,76562-68-0
L-2-(2-bromo-acetylamino)-3-phenylpropionic acid ethyl ester

: 1379456-23-1
(S)-1-methyl-3-(2-((1-(ethyloxy)-1-oxo-3-phenylpropan-2-yl)amino)-2-oxoethyl)-1H-imidazol-3-ium bromide

Guidance literature:: In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1039/c2gc16090k

Reference yield:

: 3182-93-2
(L)-phenylalanine ethyl ester hydrochloride

: 1379456-23-1
(S)-1-methyl-3-(2-((1-(ethyloxy)-1-oxo-3-phenylpropan-2-yl)amino)-2-oxoethyl)-1H-imidazol-3-ium bromide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / -78 - -20 °C / Inert atmosphere

2: tetrahydrofuran / -78 - 20 °C / Inert atmosphere

With triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c2gc16090k

Reference yield:

: 3081-24-1
H-Phe-OEt

: 1379456-23-1
(S)-1-methyl-3-(2-((1-(ethyloxy)-1-oxo-3-phenylpropan-2-yl)amino)-2-oxoethyl)-1H-imidazol-3-ium bromide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate / dichloromethane / 12 h / 0 °C / Green chemistry

2: diethyl ether / 24 h / 20 °C / Green chemistry

With sodium carbonate; In diethyl ether; dichloromethane;
DOI:10.1039/c6gc00415f