8,19-di(p-methoxyphenyl)-6,7,9,10,17,18,20,21-octahydrodibenzo-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

Base Information

Chemical Name:8,19-di(p-methoxyphenyl)-6,7,9,10,17,18,20,21-octahydrodibenzo-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane
CAS No.:82819-82-7
Molecular Formula:C₃₄H₃₈N₂O₆
Molecular Weight:570.686
Hs Code.:

8,19-di(p-methoxyphenyl)-6,7,9,10,17,18,20,21-octahydrodibenzo<b,k>-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

Synonyms:8,19-di(p-methoxyphenyl)-6,7,9,10,17,18,20,21-octahydrodibenzo-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

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Chemical Property of 8,19-di(p-methoxyphenyl)-6,7,9,10,17,18,20,21-octahydrodibenzo-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

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Technology Process of 8,19-di(p-methoxyphenyl)-6,7,9,10,17,18,20,21-octahydrodibenzo-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

There total 5 articles about 8,19-di(p-methoxyphenyl)-6,7,9,10,17,18,20,21-octahydrodibenzo-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 104-94-9
4-methoxy-aniline

: 82819-80-5
C₄₁H₄₅NO₁₁S₂

: 82819-82-7
8,19-di(p-methoxyphenyl)-6,7,9,10,17,18,20,21-octahydrodibenzo-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

Guidance literature:: With sodium hydroxide; In xylene; for 40h; Heating;

Reference yield: 35.8%

: 1448-52-8
N,N-bis(2-chloroethyl)-4-methoxybenzenamine

: 120-80-9,19481-10-8,37349-32-9
benzene-1,2-diol

: 82819-82-7
8,19-di(p-methoxyphenyl)-6,7,9,10,17,18,20,21-octahydrodibenzo-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

Guidance literature:: With sodium hydroxide; In butan-1-ol; at 110 ℃; for 18.75h;

Reference yield:

: 4792-78-3
2-(2-hydroxy-phenoxy)-ethanol

: 82819-82-7
8,19-di(p-methoxyphenyl)-6,7,9,10,17,18,20,21-octahydrodibenzo-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

Guidance literature:: Multi-step reaction with 3 steps

1: 5.2 g / sodium hydroxide, / butan-1-ol / 9 h / 115 °C

2: pyridine / 11 h / 0 - 5 °C

3: 57 percent / sodium hydroxide / xylene / 40 h / Heating

With pyridine; sodium hydroxide; In xylene; butan-1-ol;