2-[(1-hydroxymethyl)cyclohexyl]-3-trimethylsilylprop-1-en-1-yl pivalate

Base Information

Chemical Name:2-[(1-hydroxymethyl)cyclohexyl]-3-trimethylsilylprop-1-en-1-yl pivalate
CAS No.:468773-69-5
Molecular Formula:C₁₈H₃₄O₃Si
Molecular Weight:326.552
Hs Code.:

Synonyms:2-[(1-hydroxymethyl)cyclohexyl]-3-trimethylsilylprop-1-en-1-yl pivalate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[(1-hydroxymethyl)cyclohexyl]-3-trimethylsilylprop-1-en-1-yl pivalate

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Technology Process of 2-[(1-hydroxymethyl)cyclohexyl]-3-trimethylsilylprop-1-en-1-yl pivalate

There total 3 articles about 2-[(1-hydroxymethyl)cyclohexyl]-3-trimethylsilylprop-1-en-1-yl pivalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 468773-68-4
2-cyclohexylidene-3-trimethylsilylprop-1-yl pivalate

: 468773-69-5
2-[(1-hydroxymethyl)cyclohexyl]-3-trimethylsilylprop-1-en-1-yl pivalate

Guidance literature:: With diethylaluminium chloride; In hexane; dichloromethane; at -60 ℃; for 0.25h;
DOI:10.1016/S0040-4020(02)00403-9

Reference yield:

: 3282-30-2
pivaloyl chloride

: 468773-69-5
2-[(1-hydroxymethyl)cyclohexyl]-3-trimethylsilylprop-1-en-1-yl pivalate

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / pyridine / 20 °C

2: 26 percent / Et₂AlCl / CH₂Cl₂; hexane / 0.25 h / -60 °C

With diethylaluminium chloride; In pyridine; hexane; dichloromethane;
DOI:10.1016/S0040-4020(02)00403-9

Reference yield:

: 306326-67-0
2-cyclohexylidene-3-trimethylsilyl-1-propanol

: 468773-69-5
2-[(1-hydroxymethyl)cyclohexyl]-3-trimethylsilylprop-1-en-1-yl pivalate

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / pyridine / 20 °C

2: 26 percent / Et₂AlCl / CH₂Cl₂; hexane / 0.25 h / -60 °C

With diethylaluminium chloride; In pyridine; hexane; dichloromethane;
DOI:10.1016/S0040-4020(02)00403-9