Technology Process of 2-n-hexylaniline
There total 19 articles about 2-n-hexylaniline which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 85 percent / tetrakis(triphenylphosphine)palladium(0) / toluene / 15 h / 100 °C
2: nickel(II) acetate tetrahydrate; sodium borohydride / ethanol / 3 h
3: hydrochloric acid / ethanol / 10 h / Heating
With
hydrogenchloride; sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium(0); nickel diacetate;
In
ethanol; toluene;
1: Alkylation / 2: Hydrogenation / 3: Deacetylation;
DOI:10.1016/S0040-4020(99)00934-5
- Guidance literature:
-
Multi-step reaction with 2 steps
1: nickel(II) acetate tetrahydrate; sodium borohydride / ethanol / 3 h
2: hydrochloric acid / ethanol / 10 h / Heating
With
hydrogenchloride; sodium tetrahydroborate; nickel diacetate;
In
ethanol;
1: Hydrogenation / 2: Deacetylation;
DOI:10.1016/S0040-4020(99)00934-5
- Guidance literature:
-
Multi-step reaction with 4 steps
1: pyridine / CH2Cl2
2: (PPh3)4Pd / toluene / 24 h
3: H2 / Pd/C / tetrahydrofuran / 2 h
4: HCl, 5percent NaOH / ethanol
With
pyridine; hydrogenchloride; sodium hydroxide; tetrakis(triphenylphosphine) palladium(0); hydrogen;
palladium on activated charcoal;
In
tetrahydrofuran; ethanol; dichloromethane; toluene;
DOI:10.1051/jcp:1998249