2-hexylacetanilide

Base Information

Chemical Name:2-hexylacetanilide
CAS No.:83480-34-6
Molecular Formula:C₁₄H₂₁NO
Molecular Weight:219.327
Hs Code.:

Synonyms:

Suppliers and Price of 2-hexylacetanilide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-hexylacetanilide

Chemical Property:

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Technology Process of 2-hexylacetanilide

There total 4 articles about 2-hexylacetanilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 80471-76-7
2-[hex-1'-enyl]acetanilide

: 83480-34-6
2-hexylacetanilide

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; for 2h; Yield given;
DOI:10.1051/jcp:1998249

Reference yield:

: 614-76-6
N-acetyl-2-bromoaniline

: 83480-34-6
2-hexylacetanilide

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / tetrakis(triphenylphosphine)palladium⁽⁰⁾ / toluene / 15 h / 100 °C

2: nickel(II) acetate tetrahydrate; sodium borohydride / ethanol / 3 h

With sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; nickel diacetate; In ethanol; toluene; 1: Alkylation / 2: Hydrogenation;
DOI:10.1016/S0040-4020(99)00934-5

Reference yield:

: 615-36-1
2-bromoaniline

: 83480-34-6
2-hexylacetanilide

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / CH₂Cl₂

2: (PPh₃)4Pd / toluene / 24 h

3: H₂ / Pd/C / tetrahydrofuran / 2 h

With pyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; hydrogen; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1051/jcp:1998249