2-[(4-{(tert-butoxycarbonyl)[2-(2-pyridinyl)ethyl]amino}anilino)carbonyl]-4'-hydroxy-1,1'-biphenyl

Base Information

• Chemical Name: 2-[(4-{(tert-butoxycarbonyl)[2-(2-pyridinyl)ethyl]amino}anilino)carbonyl]-4'-hydroxy-1,1'-biphenyl
• CAS No.: 408366-71-2
• Molecular Formula: C₃₁H₃₁N₃O₄
• Molecular Weight: 509.605

Synonyms:2-[(4-{(tert-butoxycarbonyl)[2-(2-pyridinyl)ethyl]amino}anilino)carbonyl]-4'-hydroxy-1,1'-biphenyl

Chemical Property of 2-[(4-{(tert-butoxycarbonyl)[2-(2-pyridinyl)ethyl]amino}anilino)carbonyl]-4'-hydroxy-1,1'-biphenyl

Chemical Property:

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Technology Process of 2-[(4-{(tert-butoxycarbonyl)[2-(2-pyridinyl)ethyl]amino}anilino)carbonyl]-4'-hydroxy-1,1'-biphenyl

There total 1 articles about 2-[(4-{(tert-butoxycarbonyl)[2-(2-pyridinyl)ethyl]amino}anilino)carbonyl]-4'-hydroxy-1,1'-biphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-benzyloxy-2'-[(4-{(tert-butoxycarbonyl)[2-(2-pyridinyl)ethyl]amino}anilino)carbonyl]-1,1'-biphenyl (408366-69-8) + ethyl acetate n-hexane → 2-[(4-{(tert-butoxycarbonyl)[2-(2-pyridinyl)ethyl]amino}anilino)carbonyl]-4'-hydroxy-1,1'-biphenyl (408366-71-2)

Guidance literature:

palladium; In methanol; ethyl acetate;

Reference yield:

2-[(4-{(tert-butoxycarbonyl)[2-(2-pyridinyl)ethyl]amino}anilino)carbonyl]-4'-hydroxy-1,1'-biphenyl (408366-71-2) + ethyl acetate n-hexane + ethyl bromoacetate (105-36-2) → ethyl ({2'-[(4-{(tert-butoxycarbonyl)[2-(2-pyridinyl)ethyl]amino}anilino)carbonyl]-1,1'-biphenyl-4-yl)oxy)acetate (408366-76-7)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide;

Reference yield:

methanol-dichloromethane + 2-[(4-{(tert-butoxycarbonyl)[2-(2-pyridinyl)ethyl]amino}anilino)carbonyl]-4'-hydroxy-1,1'-biphenyl (408366-71-2) + (2-chloroethyl)dimethylamine hydrochloride (4584-46-7) → 2-[(4-{(tert-butoxycarbonyl)[2-(2-pyridinyl)ethyl]amino}anilino)-carbonyl]-4'-[2-(dimethylamino)ethoxy]-1,1'-biphenyl (408366-72-3)

Guidance literature:

With potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;

upstream raw materials:

4-benzyloxy-2'-[(4-{(tert-butoxycarbonyl)[2-(2-pyridinyl)ethyl]amino}anilino)carbonyl]-1,1'-biphenyl

Downstream raw materials:

ethyl ({2'-[(4-{(tert-butoxycarbonyl)[2-(2-pyridinyl)ethyl]amino}anilino)carbonyl]-1,1'-biphenyl-4-yl)oxy)acetate

2-[(4-{(tert-butoxycarbonyl)[2-(2-pyridinyl)ethyl]amino}anilino)carbonyl]-4'-[3-(dimethylamino)propoxy]-1,1'-biphenyl

2-[(4-{(tert-butoxycarbonyl)[2-(2-pyridinyl)ethyl]amino}anilino)-carbonyl]-4'-[2-(dimethylamino)ethoxy]-1,1'-biphenyl

2-[(4-{(tert-Butoxycarbonyl)[2-(2-pyridinyl)ethyl]amino}anilino)carbonyl]-4'-(2-methoxyethoxy)-1,1'-biphenyl

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