((CH₃)2GePC₆H₅)2CH₂CH₂

Base Information Edit

Chemical Name:((CH₃)2GePC₆H₅)2CH₂CH₂
CAS No.:81744-50-5
Molecular Formula:C₁₈H₂₆Ge₂P₂
Molecular Weight:449.532
Hs Code.:
Mol file:81744-50-5.mol

((CH<sub>3</sub>)2GePC<sub>6</sub>H<sub>5</sub>)2CH<sub>2</sub>CH<sub>2</sub>

Synonyms:((CH₃)2GePC₆H₅)2CH₂CH₂

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Chemical Property of ((CH₃)2GePC₆H₅)2CH₂CH₂ Edit

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of ((CH₃)2GePC₆H₅)2CH₂CH₂

There total 2 articles about ((CH₃)2GePC₆H₅)2CH₂CH₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82312-13-8
1-(phenylphosphino)-2-(dimethylbromogermyl)ethane

: 78665-53-9
2-dimethylgerma 1-phenyl phosphetane

: 68160-18-9
(CH₃)2GeP(C₆H₅)

: 81744-50-5
((CH₃)2GePC₆H₅)2CH₂CH₂

: 78665-55-1
trans-3,3-dimethyl-1,2-diphenyl-1,2,3-diphosphagermolane

: 82312-28-5
3,3-dimethyl-2-(dimethylphenylgermyl)-1-phenyl-1,2,3-diphosphagermolane

Guidance literature:: With dimethyl amine; In benzene; byproducts: dimethylamine hydrobromide; Ge compd. soln. stirred at -30°C, 2-fold excess of dimethylamineallowed to bubble; centrifuged, evapd. (vac.), washed with C6H6, then with pentane, distd., obtained as mixt.;

Reference yield:

: 82312-30-9
1-(phenylphosphino)-2-(dimethyl(phenylphosphino)germyl)ethane

: 3058-23-9
dimethylbis(diethylamino)germanium

: 81744-50-5
((CH₃)2GePC₆H₅)2CH₂CH₂

Guidance literature:: In benzene; solns. of educts in C6H6 added simultaneously to C6H6, refluxed for 2 h; solvent distd. (vac.); elem. anal.;

Reference yield: 75.0%

: 81744-50-5
((CH₃)2GePC₆H₅)2CH₂CH₂

: 82312-32-1
2-(dimethylgermyl)-1-(phenylphosphino)ethane

: 1449-64-5
dimethylgermane

: 638-21-1
phenylphosphane

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; Ge compd. soln. added to excess of LiAlH4 in Et2O, refluxed for 2 h; hydrolyzed, extd. (Et2O), dried (Na2SO4), distd.;