2-azido-10-(benzyloxy)-1-iododecane

Base Information

Chemical Name:2-azido-10-(benzyloxy)-1-iododecane
CAS No.:556011-31-5
Molecular Formula:C₁₇H₂₆IN₃O
Molecular Weight:415.317
Hs Code.:

Synonyms:2-azido-10-(benzyloxy)-1-iododecane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-azido-10-(benzyloxy)-1-iododecane

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Technology Process of 2-azido-10-(benzyloxy)-1-iododecane

There total 3 articles about 2-azido-10-(benzyloxy)-1-iododecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 100189-71-7
((dec-9-en-1-yloxy)methyl)benzene

: 556011-31-5
2-azido-10-(benzyloxy)-1-iododecane

Guidance literature:: With sodium azide; Iodine monochloride; In acetonitrile; at -15 - 20 ℃;
DOI:10.1002/hlca.200590119

Reference yield:

: 13019-22-2
9-Decen-1-ol

: 556011-31-5
2-azido-10-(benzyloxy)-1-iododecane

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / NaH / tetrahydrofuran / 20 °C

2: 72 percent / ICl; NaN₃ / acetonitrile / -15 - 20 °C

With sodium azide; Iodine monochloride; sodium hydride; In tetrahydrofuran; acetonitrile;
DOI:10.1002/hlca.200590119

Reference yield:

: 100-39-0
benzyl bromide

: 556011-31-5
2-azido-10-(benzyloxy)-1-iododecane

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / NaH / tetrahydrofuran / 20 °C

2: 72 percent / ICl; NaN₃ / acetonitrile / -15 - 20 °C

With sodium azide; Iodine monochloride; sodium hydride; In tetrahydrofuran; acetonitrile;
DOI:10.1002/hlca.200590119