2-methyl-2-(2-methyl-1,3-dioxolan-2-yl)-3-phenylpropanoic acid mono-(dicyclohexylammonium) salt

Base Information

Chemical Name:2-methyl-2-(2-methyl-1,3-dioxolan-2-yl)-3-phenylpropanoic acid mono-(dicyclohexylammonium) salt
CAS No.:1264295-96-6
Molecular Formula:C₁₂H₂₃N*C₁₄H₁₈O₄
Molecular Weight:431.616
Hs Code.:

Synonyms:2-methyl-2-(2-methyl-1,3-dioxolan-2-yl)-3-phenylpropanoic acid mono-(dicyclohexylammonium) salt

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Chemical Property of 2-methyl-2-(2-methyl-1,3-dioxolan-2-yl)-3-phenylpropanoic acid mono-(dicyclohexylammonium) salt

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Technology Process of 2-methyl-2-(2-methyl-1,3-dioxolan-2-yl)-3-phenylpropanoic acid mono-(dicyclohexylammonium) salt

There total 2 articles about 2-methyl-2-(2-methyl-1,3-dioxolan-2-yl)-3-phenylpropanoic acid mono-(dicyclohexylammonium) salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1264295-94-4
ethyl2-methyl-2-(2-methyl-1,3-dioxolan-2-yl)-3-phenylpropanoate

: 101-83-7
N-cyclohexyl-cyclohexanamine

: 1264295-96-6
2-methyl-2-(2-methyl-1,3-dioxolan-2-yl)-3-phenylpropanoic acid mono-(dicyclohexylammonium) salt

Guidance literature:: ethyl2-methyl-2-(2-methyl-1,3-dioxolan-2-yl)-3-phenylpropanoate; With lithium hydroxide; In ethylene glycol; at 200 ℃; for 0.5h;

With water; sodium hydroxide; In ethylene glycol;

N-cyclohexyl-cyclohexanamine;

Reference yield:

: 107449-78-5
ethyl α-methyl-α-benzylacetoacetate

: 1264295-96-6
2-methyl-2-(2-methyl-1,3-dioxolan-2-yl)-3-phenylpropanoic acid mono-(dicyclohexylammonium) salt

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid; orthoformic acid triethyl ester / 55 °C

2: lithium hydroxide / ethylene glycol / 0.5 h / 200 °C

With toluene-4-sulfonic acid; orthoformic acid triethyl ester; lithium hydroxide; In ethylene glycol;