N-[1-Dimethylcarbamoyl-1-phenyl-3-(tetrahydro-pyran-2-yloxy)-propyl]-benzamide

Base Information

• Chemical Name: N-[1-Dimethylcarbamoyl-1-phenyl-3-(tetrahydro-pyran-2-yloxy)-propyl]-benzamide
• CAS No.: 91527-84-3
• Molecular Formula: C₂₄H₃₀N₂O₄
• Molecular Weight: 410.513

Synonyms:N-[1-Dimethylcarbamoyl-1-phenyl-3-(tetrahydro-pyran-2-yloxy)-propyl]-benzamide

Chemical Property of N-[1-Dimethylcarbamoyl-1-phenyl-3-(tetrahydro-pyran-2-yloxy)-propyl]-benzamide

Chemical Property:

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Technology Process of N-[1-Dimethylcarbamoyl-1-phenyl-3-(tetrahydro-pyran-2-yloxy)-propyl]-benzamide

There total 2 articles about N-[1-Dimethylcarbamoyl-1-phenyl-3-(tetrahydro-pyran-2-yloxy)-propyl]-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

2,4-Diphenyl-4-[2-(tetrahydro-pyran-2-yloxy)-ethyl]-4H-oxazol-5-one (91527-87-6) + dimethyl amine (124-40-3) → N-[1-Dimethylcarbamoyl-1-phenyl-3-(tetrahydro-pyran-2-yloxy)-propyl]-benzamide (91527-84-3)

Guidance literature:

In acetonitrile;

DOI:10.1016/S0040-4039(01)81153-9

Reference yield:

2,4-diphenyl-4H-oxazol-5-one (28687-81-2,719263-73-7) → N-[1-Dimethylcarbamoyl-1-phenyl-3-(tetrahydro-pyran-2-yloxy)-propyl]-benzamide (91527-84-3)

Guidance literature:

Multi-step reaction with 2 steps

1: ((CH₃)2CH)2NCH₂CH₃ / acetonitrile / Heating

2: 40 percent / acetonitrile

With N-ethyl-N,N-diisopropylamine; In acetonitrile;

DOI:10.1016/S0040-4039(01)81153-9

Reference yield: 90.0%

N-[1-Dimethylcarbamoyl-1-phenyl-3-(tetrahydro-pyran-2-yloxy)-propyl]-benzamide (91527-84-3) → N-(1-Dimethylcarbamoyl-3-hydroxy-1-phenyl-propyl)-benzamide (91527-81-0)

Guidance literature:

With pyridinium p-toluenesulfonate; In ethanol; at 80 ℃;

DOI:10.1016/S0040-4039(01)81153-9

upstream raw materials:

2,4-Diphenyl-4-[2-(tetrahydro-pyran-2-yloxy)-ethyl]-4H-oxazol-5-one

dimethyl amine

2,4-diphenyl-4H-oxazol-5-one

Downstream raw materials:

N-(1-Dimethylcarbamoyl-3-hydroxy-1-phenyl-propyl)-benzamide

N-(2-Oxo-3-phenyl-tetrahydro-furan-3-yl)-benzamide

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