2-chlorophenyl 4-nitrobenzoate

Base Information

• Chemical Name: 2-chlorophenyl 4-nitrobenzoate
• CAS No.: 85965-91-9
• Molecular Formula: C13H8 Cl N O4
• Molecular Weight: 277.6599

Synonyms:Phenol,o-chloro-, p-nitrobenzoate (6CI); 2-Chlorophenyl 4-nitrobenzoate; NSC 6894;o-Chlorophenol p-nitrobenzoate

Chemical Property of 2-chlorophenyl 4-nitrobenzoate

Chemical Property:

• Vapor Pressure: 4.3E-09mmHg at 25°C
• Boiling Point: 472.4°Cat760mmHg
• Flash Point: 239.5°C
• Density: 1.412g/cm³

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-chlorophenyl 4-nitrobenzoate

There total 2 articles about 2-chlorophenyl 4-nitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

2-monochlorophenol (95-57-8) + 4-nitro-benzoic acid (62-23-7) → 2-chlorophenyl 4-nitrobenzoate (85965-91-9)

Guidance literature:

With potassium carbonate; In ethyl acetate; for 0.5h; Heating;

DOI:10.1016/j.tet.2007.10.011

Reference yield:

2-monochlorophenol (95-57-8) + 4-nitro-benzoyl chloride (122-04-3) → 2-chlorophenyl 4-nitrobenzoate (85965-91-9)

Guidance literature:

With pyridine;

Reference yield:

2-chlorophenyl 4-nitrobenzoate (85965-91-9) → 3-chloro-4-hydroxy-4'-nitro-benzophenone (99768-27-1)

Guidance literature:

With aluminium trichloride;

upstream raw materials:

2-monochlorophenol

4-nitro-benzoyl chloride

4-nitro-benzoic acid

Downstream raw materials:

3-chloro-4-hydroxy-4'-nitro-benzophenone

3-chloro-4-methoxy-4'-nitro-benzophenone

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