trithioboric acid triphenyl ester

Base Information

Chemical Name:trithioboric acid triphenyl ester
CAS No.:1041-16-3
Molecular Formula:C₁₈H₁₅BS₃
Molecular Weight:338.326
Hs Code.:

Synonyms:trithioboric acid triphenyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trithioboric acid triphenyl ester

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Technology Process of trithioboric acid triphenyl ester

There total 8 articles about trithioboric acid triphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

: 108-98-5
thiophenol

: 1041-16-3
trithioboric acid triphenyl ester

Guidance literature:: With boron trichloride; In n-heptane; at 0 - 50 ℃; for 14h; Inert atmosphere;
DOI:10.1021/ja905287q

Reference yield: 19.0%

: 10294-34-5
boron trichloride

: 108-98-5
thiophenol

: 1041-16-3
trithioboric acid triphenyl ester

Guidance literature:: In n-heptane; (N2); C6H5SH added to BCl3 in heptane at 0°C, warmed to room temp. over 1 h, stirred for 1 h, heated at 50°C for 12 h; evapd. (vac.), washed (ether), dried (vac.);
DOI:10.1021/ja905287q