N-<1(S)-(ethoxycarbonyl)-3-phenylpropyl>-(RS)-carbobenzyloxyalanine N-oxysuccinimidyl ester

Base Information

Chemical Name:N-<1(S)-(ethoxycarbonyl)-3-phenylpropyl>-(RS)-carbobenzyloxyalanine N-oxysuccinimidyl ester
CAS No.:97998-67-9
Molecular Formula:C₂₇H₃₀N₂O₈
Molecular Weight:510.544
Hs Code.:

Synonyms:N-<1(S)-(ethoxycarbonyl)-3-phenylpropyl>-(RS)-carbobenzyloxyalanine N-oxysuccinimidyl ester

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Chemical Property of N-<1(S)-(ethoxycarbonyl)-3-phenylpropyl>-(RS)-carbobenzyloxyalanine N-oxysuccinimidyl ester

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Technology Process of N-<1(S)-(ethoxycarbonyl)-3-phenylpropyl>-(RS)-carbobenzyloxyalanine N-oxysuccinimidyl ester

There total 4 articles about N-<1(S)-(ethoxycarbonyl)-3-phenylpropyl>-(RS)-carbobenzyloxyalanine N-oxysuccinimidyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 943-73-7
D-homophenylalanine

: 97998-67-9
N-<1(S)-(ethoxycarbonyl)-3-phenylpropyl>-(RS)-carbobenzyloxyalanine N-oxysuccinimidyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / HCl / 2 h / Heating

2: NaOH, H₂ / 5percent Pd/C / ethanol / 25 °C / 2172.02 - 4654.3 Torr

3: Et₃N / dimethylformamide / 2 h / 25 °C

4: DCC / 1,2-dimethoxy-ethane / 24 h / 0 °C

With hydrogenchloride; sodium hydroxide; hydrogen; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In 1,2-dimethoxyethane; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00149a009

Reference yield:

: 90891-21-7
L-(+)-α-amino-4-phenylbutyric acid ethyl ester hydrochloride

: 97998-67-9
N-<1(S)-(ethoxycarbonyl)-3-phenylpropyl>-(RS)-carbobenzyloxyalanine N-oxysuccinimidyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: NaOH, H₂ / 5percent Pd/C / ethanol / 25 °C / 2172.02 - 4654.3 Torr

2: Et₃N / dimethylformamide / 2 h / 25 °C

3: DCC / 1,2-dimethoxy-ethane / 24 h / 0 °C

With sodium hydroxide; hydrogen; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In 1,2-dimethoxyethane; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00149a009