1-(phenylmethyl) hydrogen tetrahydro-2-nitrosopyridazine-1,(3S)(2H)-dicarboxylate

Base Information

Chemical Name:1-(phenylmethyl) hydrogen tetrahydro-2-nitrosopyridazine-1,(3S)(2H)-dicarboxylate
CAS No.:1161076-91-0
Molecular Formula:C₁₃H₁₅N₃O₅
Molecular Weight:293.279
Hs Code.:

Synonyms:1-(phenylmethyl) hydrogen tetrahydro-2-nitrosopyridazine-1,(3S)(2H)-dicarboxylate

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Chemical Property of 1-(phenylmethyl) hydrogen tetrahydro-2-nitrosopyridazine-1,(3S)(2H)-dicarboxylate

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Technology Process of 1-(phenylmethyl) hydrogen tetrahydro-2-nitrosopyridazine-1,(3S)(2H)-dicarboxylate

There total 1 articles about 1-(phenylmethyl) hydrogen tetrahydro-2-nitrosopyridazine-1,(3S)(2H)-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 65632-62-4
(3S)-hexahydro-1,3-pridazinedicarboxylic acid 1-(phenylmethyl) ester

: 1161076-91-0
1-(phenylmethyl) hydrogen tetrahydro-2-nitrosopyridazine-1,(3S)(2H)-dicarboxylate

Guidance literature:: With hydrogenchloride; sodium nitrite; In water; at 4 ℃; for 3.5h;

Reference yield:

: 1161076-91-0
1-(phenylmethyl) hydrogen tetrahydro-2-nitrosopyridazine-1,(3S)(2H)-dicarboxylate

: 1161076-92-1
4,5,6,7-tetrahydro-3-hydroxy-7-[(phenylmethoxy)carbonyl][1,2,3]oxadiazolo[3,4-b]pyridazin-8-ium inner salt

Guidance literature:: With trifluoroacetic anhydride; In diethyl ether; at 0 - 2 ℃; for 3.5h;

Reference yield:

: 1161076-91-0
1-(phenylmethyl) hydrogen tetrahydro-2-nitrosopyridazine-1,(3S)(2H)-dicarboxylate

: 1161076-93-2
phenylmethyl 3-[2-(cyclopropylamino)-4-pyrimidinyl]-2-(4-fluorophenyl)-5,6-dihydropyrazolo[1,5-b]pyridazine-7(4H)-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: trifluoroacetic anhydride / diethyl ether / 3.5 h / 0 - 2 °C

2: 1,3,5-trimethyl-benzene / 4 h / 140 °C

3: chloroform / 1.08 h / 120 - 160 °C / Sealed tube; Microwave irradiation

With trifluoroacetic anhydride; In diethyl ether; chloroform; 1,3,5-trimethyl-benzene;