2-((2,6-Dichlorophenyl)amino)benzaldehyde

Base Information

Chemical Name:2-((2,6-Dichlorophenyl)amino)benzaldehyde
CAS No.:22121-58-0
Molecular Formula:C13H9 Cl2 N O
Molecular Weight:266.127
Hs Code.:2922399090
European Community (EC) Number:641-594-7
UNII:9218J5N522
DSSTox Substance ID:DTXSID90176642
Nikkaji Number:J29.883B
Wikidata:Q27271451
Mol file:22121-58-0.mol

Synonyms:22121-58-0;2-((2,6-Dichlorophenyl)amino)benzaldehyde;2-(2,6-Dichloroanilino)benzaldehyde;Diclofenac impurity B;2-[(2,6-DICHLOROPHENYL)AMINO]BENZALDEHYDE;o-(2,6-Dichloroanilino)benzaldehyde;2-(2,6-Dichloroanilino) benzaldehyde;Anthranilaldehyde, N-(2,6-dichlorophenyl)-;2-[(2,6-Dichlorophenyl)amino]benzaldehyde (Diclofenac impurity);Benzaldehyde, 2-((2,6-dichlorophenyl)amino)-;9218J5N522;Benzaldehyde, 2-[(2,6-dichlorophenyl)amino]-;UNII-9218J5N522;Diclofenac sodium impurity B [EP];Diclofenac potassium impurity B [EP];N-(2,6-Dichlorophenyl)anthranilaldehyde;Diclofenac sodium specified impurity B [EP];Diclofenac potassium specified impurity B [EP];SCHEMBL2553022;DTXSID90176642;MILOIOYXRHLAAH-UHFFFAOYSA-N;MFCD03788574;AKOS027447593;(2,6-dichloro-phenylamino)-benz-aldehyde;BS-52040;[2-(2,6-Dichlorophenyl)amino]benzaldehyde;CS-0156692;FT-0666597;NS00003337;D83566;A899533;DICLOFENAC SODIUM IMPURITY B [EP IMPURITY];DICLOFENAC POTASSIUM IMPURITY B [EP IMPURITY];Q27271451;2-[(2,6-Dichlorophenyl)amino]benzaldehyde, pharmaceutical impurity standard

Suppliers and Price of 2-((2,6-Dichlorophenyl)amino)benzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-[(2,6-Dichlorophenyl)amino]benzaldehyde(Diclofenacimpurity)
5mg
$ 205.00

TRC
2-[(2,6-Dichlorophenyl)amino]benzaldehyde(Diclofenacimpurity)
10mg
$ 320.00

Sigma-Aldrich
2-[(2,6-Dichlorophenyl)amino]benzaldehyde pharmaceuticalimpuritystandard
50 mg
$ 338.00

Biosynth Carbosynth
Diclofenac impurity B
25 mg
$ 175.00

Biosynth Carbosynth
Diclofenac impurity B
10 mg
$ 80.00

Biosynth Carbosynth
Diclofenac impurity B
5 mg
$ 50.00

Biosynth Carbosynth
Diclofenac impurity B
50 mg
$ 300.00

Biosynth Carbosynth
Diclofenac impurity B
100 mg
$ 500.00

American Custom Chemicals Corporation
[2-[(2,6-DICHLOROPHENYL)AMINO]BENZALDEHYDE 95.00%
10MG
$ 1871.10

American Custom Chemicals Corporation
[2-[(2,6-DICHLOROPHENYL)AMINO]BENZALDEHYDE 95.00%
1MG
$ 315.00

Total 18 raw suppliers

Chemical Property of 2-((2,6-Dichlorophenyl)amino)benzaldehyde

Chemical Property:

Melting Point:112-114?C
Boiling Point:349.0±42.0 °C(Predicted)
PKA:-4.46±0.50(Predicted)
PSA：29.10000
Density:1.392±0.06 g/cm3(Predicted)
LogP:4.62250
Storage Temp.:-20°C Freezer, Under Inert Atmosphere
Solubility.:Chloroform (Slightly), Methanol (Slightly, Heated
XLogP3:4.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:265.0061193
Heavy Atom Count:17
Complexity:252

Purity/Quality:

99%, ^*data from raw suppliers

2-[(2,6-Dichlorophenyl)amino]benzaldehyde(Diclofenacimpurity) ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)C=O)NC2=C(C=CC=C2Cl)Cl
Uses An impurity of Diclofenac (D436450) 2-[(2,6-Dichlorophenyl)amino]benzaldehyde (Diclofenac EP Impurity B) is an impurity of Diclofenac (D436450). Diclofenac impurity. Anti-inflammatory

Technology Process of 2-((2,6-Dichlorophenyl)amino)benzaldehyde

There total 3 articles about 2-((2,6-Dichlorophenyl)amino)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 15307-79-6
diclofenac sodium

: 22121-58-0
2-[(2,6-dichlorophenyl)amino]benzaldehyde

Guidance literature:: With iron(III) chloride; oxygen; In N,N-dimethyl-formamide; at 110 ℃;
DOI:10.1039/d0ob01790f

Reference yield:

: 67-56-1
methanol

: 15307-79-6
diclofenac sodium

: 15362-40-0
1-(2,6-dichlorophenyl)indolin-2-one

: 22121-58-0
2-[(2,6-dichlorophenyl)amino]benzaldehyde

: 15307-78-5
2-[(2,6-dichlorophenyl)amino]phenylacetic acid methyl ester

Guidance literature:: With water; at 19.85 ℃; for 17532h; Further Variations:; rel. humidity; complexed with β-cyclodextrin; Kinetics; Product distribution;