3-<<4-(2-methoxyphenyl)piperazine-1-yl>methyl>-5-methoxy-2,3-dihydroimidazo<1,2-c>quinazoline

Base Information

Chemical Name:3-<<4-(2-methoxyphenyl)piperazine-1-yl>methyl>-5-methoxy-2,3-dihydroimidazo<1,2-c>quinazoline
CAS No.:149847-83-6
Molecular Formula:C₂₃H₂₇N₅O₂
Molecular Weight:405.5
Hs Code.:

Synonyms:3-<<4-(2-methoxyphenyl)piperazine-1-yl>methyl>-5-methoxy-2,3-dihydroimidazo<1,2-c>quinazoline

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Chemical Property of 3-<<4-(2-methoxyphenyl)piperazine-1-yl>methyl>-5-methoxy-2,3-dihydroimidazo<1,2-c>quinazoline

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Technology Process of 3-<<4-(2-methoxyphenyl)piperazine-1-yl>methyl>-5-methoxy-2,3-dihydroimidazo<1,2-c>quinazoline

There total 1 articles about 3-<<4-(2-methoxyphenyl)piperazine-1-yl>methyl>-5-methoxy-2,3-dihydroimidazo<1,2-c>quinazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 67-56-1
methanol

: 149847-79-0
DL 017

: 149847-83-6
3-<<4-(2-methoxyphenyl)piperazine-1-yl>methyl>-5-methoxy-2,3-dihydroimidazo<1,2-c>quinazoline

Guidance literature:: With sodium hydroxide; at 55 ℃; for 48h;
DOI:10.1021/jm00067a017

Reference yield: 34.0%

: 149847-83-6
3-<<4-(2-methoxyphenyl)piperazine-1-yl>methyl>-5-methoxy-2,3-dihydroimidazo<1,2-c>quinazoline

: DC 015

Guidance literature:: With sodium hydroxide; In methanol; for 6h; Heating;
DOI:10.1021/jm00067a017

Reference yield:

: 149847-83-6
3-<<4-(2-methoxyphenyl)piperazine-1-yl>methyl>-5-methoxy-2,3-dihydroimidazo<1,2-c>quinazoline

: 3-<<4-(2-methoxyphenyl)piperazin-1-yl>methyl>-6-methyl-2,3-dihydroimidazo<1,2-c>quinazolin-5(6H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: 34 percent / NaOH / methanol / 6 h / Heating

2: 1.) NaH / 1.) DMF, 0 deg C, 20 min, 2.) DMF, 24 h

With sodium hydroxide; sodium hydride; In methanol;
DOI:10.1021/jm00067a017