6-[(ethoxy)(trimethylsilanyloxy)methylidene]-3-methyl-1-(trimethylsilanyloxy)cyclohexene

Base Information

• Chemical Name: 6-[(ethoxy)(trimethylsilanyloxy)methylidene]-3-methyl-1-(trimethylsilanyloxy)cyclohexene
• CAS No.: 394250-96-5
• Molecular Formula: C₁₆H₃₂O₃Si₂
• Molecular Weight: 328.599

Synonyms:6-[(ethoxy)(trimethylsilanyloxy)methylidene]-3-methyl-1-(trimethylsilanyloxy)cyclohexene

Chemical Property of 6-[(ethoxy)(trimethylsilanyloxy)methylidene]-3-methyl-1-(trimethylsilanyloxy)cyclohexene

Chemical Property:

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Technology Process of 6-[(ethoxy)(trimethylsilanyloxy)methylidene]-3-methyl-1-(trimethylsilanyloxy)cyclohexene

There total 1 articles about 6-[(ethoxy)(trimethylsilanyloxy)methylidene]-3-methyl-1-(trimethylsilanyloxy)cyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

chloro-trimethyl-silane (75-77-4) + ethyl 4-methyl-2-cyclohexanone-1-carboxylate (13537-82-1) → 6-[(ethoxy)(trimethylsilanyloxy)methylidene]-3-methyl-1-(trimethylsilanyloxy)cyclohexene (394250-96-5)

Guidance literature:

With diisopropylamine; lithium diisopropyl amide; In tetrahydrofuran; hexane; at 0 ℃; for 3h;

DOI:10.1002/1099-0690(200110)2001:19<3657::AID-EJOC3657>3.0.CO;2-5

Reference yield: 96.0%

azidoacetaldehyde dimethyl acetal (114790-46-4) + 6-[(ethoxy)(trimethylsilanyloxy)methylidene]-3-methyl-1-(trimethylsilanyloxy)cyclohexene (394250-96-5) → 3-(2-azido-1-methoxyethyl)-4-methyl-2-oxo-cyclohexanecarboxylic acid ethyl ester

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 - 20 ℃; for 19h;

DOI:10.1021/jo047856x

Reference yield: 86.0%

chloroacetaldehyde dimethyl acetal (97-97-2) + 6-[(ethoxy)(trimethylsilanyloxy)methylidene]-3-methyl-1-(trimethylsilanyloxy)cyclohexene (394250-96-5) → (R)-3-((S)-2-Chloro-1-methoxy-ethyl)-4-methyl-2-oxo-cyclohexanecarboxylic acid ethyl ester

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 - 20 ℃;

DOI:10.1002/ejoc.200400805

upstream raw materials:

chloro-trimethyl-silane

ethyl 4-methyl-2-cyclohexanone-1-carboxylate

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