tert-butyl (3R)-2-benzoyl-3-methyl-5-oxo-5-(2-thioxothiazolidin-3-yl)pentanoate

Base Information

Chemical Name:tert-butyl (3R)-2-benzoyl-3-methyl-5-oxo-5-(2-thioxothiazolidin-3-yl)pentanoate
CAS No.:864515-95-7
Molecular Formula:C₂₀H₂₅NO₄S₂
Molecular Weight:407.555
Hs Code.:

Synonyms:tert-butyl (3R)-2-benzoyl-3-methyl-5-oxo-5-(2-thioxothiazolidin-3-yl)pentanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl (3R)-2-benzoyl-3-methyl-5-oxo-5-(2-thioxothiazolidin-3-yl)pentanoate

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Technology Process of tert-butyl (3R)-2-benzoyl-3-methyl-5-oxo-5-(2-thioxothiazolidin-3-yl)pentanoate

There total 1 articles about tert-butyl (3R)-2-benzoyl-3-methyl-5-oxo-5-(2-thioxothiazolidin-3-yl)pentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54441-66-6
tert-butyl benzoylacetate

: (E)-1-(2-thioxothiazolidin-3-yl)but-2-en-1-one

: 864515-95-7
tert-butyl (3R)-2-benzoyl-3-methyl-5-oxo-5-(2-thioxothiazolidin-3-yl)pentanoate

: tert-butyl (3S)-2-benzoyl-3-methyl-5-oxo-5-(2-thioxothiazolidin-3-yl)pentanoate

Guidance literature:: With [Ni((S)-Tol-BINAP)](BF₄)2; In ethyl acetate; at 0 ℃; for 12h; Title compound not separated from byproducts;
DOI:10.1021/ja053820q

Reference yield:

: 864515-95-7
tert-butyl (3R)-2-benzoyl-3-methyl-5-oxo-5-(2-thioxothiazolidin-3-yl)pentanoate

: tert-butyl (R)-4-methyl-6-oxo-2-phenyl-5,6-dihydro-4H-pyran-3-carboxylate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 ℃;
DOI:10.1021/ja053820q

Reference yield:

: 864515-95-7
tert-butyl (3R)-2-benzoyl-3-methyl-5-oxo-5-(2-thioxothiazolidin-3-yl)pentanoate

: 67-56-1
methanol

: (S)-3-methyl-5-oxo-5-phenyl-pentanoic acid methyl ester

Guidance literature:: tert-butyl (3R)-2-benzoyl-3-methyl-5-oxo-5-(2-thioxothiazolidin-3-yl)pentanoate; methanol; With potassium carbonate; In ethyl acetate;

With toluene-4-sulfonic acid; In benzene; for 2h; Heating;
DOI:10.1021/ja053820q