C₁₆H₁₈O₅

Base Information

Chemical Name:C₁₆H₁₈O₅
CAS No.:1388152-90-6
Molecular Formula:C₁₆H₁₈O₅
Molecular Weight:290.316
Hs Code.:

C<sub>16</sub>H<sub>18</sub>O<sub>5</sub>

Synonyms:C₁₆H₁₈O₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₆H₁₈O₅

Chemical Property:

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Technology Process of C₁₆H₁₈O₅

There total 6 articles about C₁₆H₁₈O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 67-56-1
methanol

: 201230-82-2
carbon monoxide

: 1388152-89-3
C₁₄H₁₆O₄

: 1388152-90-6
C₁₆H₁₈O₅

Guidance literature:: C₁₄H₁₆O₄; With N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane; chlorophosphoric acid diphenyl ester; In tetrahydrofuran; at -78 ℃; for 0.75h;

methanol; carbon monoxide; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In N,N-dimethyl-formamide; at 50 ℃; for 0.666667h;
DOI:10.1002/chem.201204303

Reference yield:

: 67-56-1
methanol

: 201230-82-2
carbon monoxide

: 1388153-22-7
C₂₆H₂₅O₇P

: 1388152-90-6
C₁₆H₁₈O₅

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In N,N-dimethyl-formamide; at 50 ℃; for 0.666667h;
DOI:10.1021/ja305864z

Reference yield:

: 1388152-88-2
C₁₄H₂₀O₄

: 1388152-90-6
C₁₆H₁₈O₅

Guidance literature:: Multi-step reaction with 3 steps

1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane / 20 °C

2: N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.75 h / -78 °C

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / N,N-dimethyl-formamide / 0.67 h / 50 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; potassium hexamethylsilazane; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja305864z