(R)-tert-butyl (1-((2-(hydroxymethyl)benzyl)oxy)pent-4-en-2-yl)carbamate

Base Information

Chemical Name:(R)-tert-butyl (1-((2-(hydroxymethyl)benzyl)oxy)pent-4-en-2-yl)carbamate
CAS No.:1333115-19-7
Molecular Formula:C₁₈H₂₇NO₄
Molecular Weight:321.417
Hs Code.:

Synonyms:(R)-tert-butyl (1-((2-(hydroxymethyl)benzyl)oxy)pent-4-en-2-yl)carbamate

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Chemical Property of (R)-tert-butyl (1-((2-(hydroxymethyl)benzyl)oxy)pent-4-en-2-yl)carbamate

Chemical Property:

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Technology Process of (R)-tert-butyl (1-((2-(hydroxymethyl)benzyl)oxy)pent-4-en-2-yl)carbamate

There total 8 articles about (R)-tert-butyl (1-((2-(hydroxymethyl)benzyl)oxy)pent-4-en-2-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1333115-18-6
(R)-methyl 2-(((2-((tert-butoxycarbonyl)amino)pent-4-en-1-yl)oxy)methyl)benzoate

: 1333115-19-7
(R)-tert-butyl (1-((2-(hydroxymethyl)benzyl)oxy)pent-4-en-2-yl)carbamate

Guidance literature:: (R)-methyl 2-(((2-((tert-butoxycarbonyl)amino)pent-4-en-1-yl)oxy)methyl)benzoate; With sodium tetrahydroborate; calcium chloride; In tetrahydrofuran; ethanol; at 20 ℃; for 17h; Inert atmosphere; Cooling with ice;

With water; sodium carbonate; In tetrahydrofuran; ethanol;

Reference yield:

: 54594-06-8
D-allylglycine

: 1333115-19-7
(R)-tert-butyl (1-((2-(hydroxymethyl)benzyl)oxy)pent-4-en-2-yl)carbamate

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogenchloride / 70 °C

2: triethylamine / dichloromethane / 1 h / 20 °C

3: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere; Cooling with ice

4: sodium hydride / tetrahydrofuran; mineral oil / 2 h / 20 °C / Inert atmosphere; Cooling with ice

5: sodium tetrahydroborate; calcium chloride / tetrahydrofuran; ethanol / 17 h / 20 °C / Inert atmosphere; Cooling with ice

With hydrogenchloride; sodium tetrahydroborate; lithium aluminium tetrahydride; sodium hydride; triethylamine; calcium chloride; In tetrahydrofuran; ethanol; dichloromethane; mineral oil;

Reference yield:

: 118-90-1
ortho-methylbenzoic acid

: 1333115-19-7
(R)-tert-butyl (1-((2-(hydroxymethyl)benzyl)oxy)pent-4-en-2-yl)carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride / 70 °C

2: N-Bromosuccinimide / 2,2'-azobis(isobutyronitrile) / tetrachloromethane / Reflux

3: sodium hydride / tetrahydrofuran; mineral oil / 2 h / 20 °C / Inert atmosphere; Cooling with ice

4: sodium tetrahydroborate; calcium chloride / tetrahydrofuran; ethanol / 17 h / 20 °C / Inert atmosphere; Cooling with ice

With hydrogenchloride; sodium tetrahydroborate; N-Bromosuccinimide; sodium hydride; calcium chloride; 2,2'-azobis(isobutyronitrile); In tetrahydrofuran; tetrachloromethane; ethanol; mineral oil;