C₄₅H₆₁NO₁₆

Base Information

Chemical Name:C₄₅H₆₁NO₁₆
CAS No.:1269040-79-0
Molecular Formula:C₄₅H₆₁NO₁₆
Molecular Weight:871.976
Hs Code.:

C<sub>45</sub>H<sub>61</sub>NO<sub>16</sub>

Synonyms:C₄₅H₆₁NO₁₆

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Chemical Property of C₄₅H₆₁NO₁₆

Chemical Property:

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Technology Process of C₄₅H₆₁NO₁₆

There total 10 articles about C₄₅H₆₁NO₁₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₆H₆₅NO₁₇

: 1269040-79-0
C₄₅H₆₁NO₁₆

Guidance literature:: With sodium periodate; In tetrahydrofuran; water; at 20 ℃; for 2.5h;

Reference yield:

: 92950-45-3
10-dehydro 10-deacetyl 7-epibaccatin V

: 1269040-79-0
C₄₅H₆₁NO₁₆

Guidance literature:: Multi-step reaction with 9 steps

1.1: pyridine / -20 - 5.8 °C / Inert atmosphere

1.2: -17.5 - 20 °C

2.1: lithium borohydride / ethanol; tetrahydrofuran / -12 - 15 °C / Inert atmosphere

2.2: -10.8 - -3 °C

3.1: dmap; triethylamine / Isopropyl acetate / 3 h / 35 °C / Inert atmosphere

3.2: 0.25 h / 19.7 °C

4.1: water / acetic acid / methanol / 9 h / 50 - 55 °C

5.1: trifluoroacetic acid / toluene / -15 °C

5.2: 0.25 h / 5 °C / pH > 5

6.1: dmap; pivaloyl chloride; 4-methyl-morpholine / tetrahydrofuran / 38 °C / Inert atmosphere

7.1: hydrogenchloride / tetrahydrofuran; methanol / 2 h / 2 °C / pH 1.5 - 1.9

8.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; tert-butyl alcohol; tetrahydrofuran / 72 h / 20 °C

8.2: florosil / 0.17 h

9.1: sodium periodate / water; tetrahydrofuran / 2.5 h / 20 °C

With 4-methyl-morpholine; pyridine; hydrogenchloride; dmap; sodium periodate; osmium(VIII) oxide; lithium borohydride; water; pivaloyl chloride; 4-methylmorpholine N-oxide; triethylamine; trifluoroacetic acid; acetic acid; In tetrahydrofuran; methanol; ethanol; Isopropyl acetate; water; toluene; tert-butyl alcohol;

Reference yield:

: 943239-53-0
C₄₁H₆₆O₁₀Si₂

: 1269040-79-0
C₄₅H₆₁NO₁₆

Guidance literature:: Multi-step reaction with 7 steps

1.1: dmap; triethylamine / Isopropyl acetate / 3 h / 35 °C / Inert atmosphere

1.2: 0.25 h / 19.7 °C

2.1: water / acetic acid / methanol / 9 h / 50 - 55 °C

3.1: trifluoroacetic acid / toluene / -15 °C

3.2: 0.25 h / 5 °C / pH > 5

4.1: dmap; pivaloyl chloride; 4-methyl-morpholine / tetrahydrofuran / 38 °C / Inert atmosphere

5.1: hydrogenchloride / tetrahydrofuran; methanol / 2 h / 2 °C / pH 1.5 - 1.9

6.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; tert-butyl alcohol; tetrahydrofuran / 72 h / 20 °C

6.2: florosil / 0.17 h

7.1: sodium periodate / water; tetrahydrofuran / 2.5 h / 20 °C

With 4-methyl-morpholine; hydrogenchloride; dmap; sodium periodate; osmium(VIII) oxide; water; pivaloyl chloride; 4-methylmorpholine N-oxide; triethylamine; trifluoroacetic acid; acetic acid; In tetrahydrofuran; methanol; Isopropyl acetate; water; toluene; tert-butyl alcohol;