1-O-(tert-butyldimethylsilyl)-3-(2'-(2''-(2''-Boc-aminoethoxy)ethoxycarbonyloxy)-4',6'-dimethylphenyl)-3,3-dimethylpropanol

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Chemical Name:1-O-(tert-butyldimethylsilyl)-3-(2'-(2''-(2''-Boc-aminoethoxy)ethoxycarbonyloxy)-4',6'-dimethylphenyl)-3,3-dimethylpropanol
CAS No.:261364-64-1
Molecular Formula:C₂₉H₅₁NO₇Si
Molecular Weight:553.812
Hs Code.:

Synonyms:1-O-(tert-butyldimethylsilyl)-3-(2'-(2''-(2''-Boc-aminoethoxy)ethoxycarbonyloxy)-4',6'-dimethylphenyl)-3,3-dimethylpropanol

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Chemical Property of 1-O-(tert-butyldimethylsilyl)-3-(2'-(2''-(2''-Boc-aminoethoxy)ethoxycarbonyloxy)-4',6'-dimethylphenyl)-3,3-dimethylpropanol

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Technology Process of 1-O-(tert-butyldimethylsilyl)-3-(2'-(2''-(2''-Boc-aminoethoxy)ethoxycarbonyloxy)-4',6'-dimethylphenyl)-3,3-dimethylpropanol

There total 3 articles about 1-O-(tert-butyldimethylsilyl)-3-(2'-(2''-(2''-Boc-aminoethoxy)ethoxycarbonyloxy)-4',6'-dimethylphenyl)-3,3-dimethylpropanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: 134098-64-9
2‐{3‐[(O‐tert‐butyldimethylsilyl)hydroxy]‐1,1‐dimethylpropyl}‐3,5‐dimethylphenol

: 261364-63-0
tert-butyl (2-(2-((((2,5-dioxopyrrolidin-1-yl)oxy)carbonyl)oxy)ethoxy)ethyl)carbamate

: 261364-64-1
1-O-(tert-butyldimethylsilyl)-3-(2'-(2''-(2''-Boc-aminoethoxy)ethoxycarbonyloxy)-4',6'-dimethylphenyl)-3,3-dimethylpropanol

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In chloroform; Heating;
DOI:10.1021/jm990498j

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 261364-64-1
1-O-(tert-butyldimethylsilyl)-3-(2'-(2''-(2''-Boc-aminoethoxy)ethoxycarbonyloxy)-4',6'-dimethylphenyl)-3,3-dimethylpropanol

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / CHCl₃ / 1.5 h / 20 °C

2: 96 percent / pyridine / CHCl₃ / 25 - 30 °C

3: 28 percent / diisopropylethylamine / CHCl₃ / Heating

With pyridine; N-ethyl-N,N-diisopropylamine; In chloroform; 1: Acylation / 2: Acylation / 3: Condensation;
DOI:10.1021/jm990498j

Reference yield:

: 139115-91-6
2-(2-tert-butyloxycarbonylaminoethoxy)ethanol

: 261364-64-1
1-O-(tert-butyldimethylsilyl)-3-(2'-(2''-(2''-Boc-aminoethoxy)ethoxycarbonyloxy)-4',6'-dimethylphenyl)-3,3-dimethylpropanol

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / pyridine / CHCl₃ / 25 - 30 °C

2: 28 percent / diisopropylethylamine / CHCl₃ / Heating

With pyridine; N-ethyl-N,N-diisopropylamine; In chloroform; 1: Acylation / 2: Condensation;
DOI:10.1021/jm990498j