7-(4-phenylthiazol-2-yl)naphthalen-2-ylamine

Base Information

Chemical Name:7-(4-phenylthiazol-2-yl)naphthalen-2-ylamine
CAS No.:1613317-36-4
Molecular Formula:C₁₉H₁₄N₂S
Molecular Weight:302.4
Hs Code.:

Synonyms:7-(4-phenylthiazol-2-yl)naphthalen-2-ylamine

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Chemical Property of 7-(4-phenylthiazol-2-yl)naphthalen-2-ylamine

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Technology Process of 7-(4-phenylthiazol-2-yl)naphthalen-2-ylamine

There total 7 articles about 7-(4-phenylthiazol-2-yl)naphthalen-2-ylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1613317-35-3
[7-(4-phenylthiazol-2-yl)naphthalen-2-yl]carbamic acid tert-butyl ester

: 1613317-36-4
7-(4-phenylthiazol-2-yl)naphthalen-2-ylamine

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; dichloromethane; at 20 ℃; for 6h; Inert atmosphere;

Reference yield:

: 1613219-39-8
7-(4-phenylthiazol-2-yl)-naphthalene-2-carboxylic acid

: 1613317-36-4
7-(4-phenylthiazol-2-yl)naphthalen-2-ylamine

Guidance literature:: Multi-step reaction with 2 steps

1: diphenyl phosphoryl azide; triethylamine / 1 h / 120 °C / Sealed tube; Microwave irradiation; Inert atmosphere

2: hydrogenchloride / dichloromethane; 1,4-dioxane / 6 h / 20 °C / Inert atmosphere

With hydrogenchloride; diphenyl phosphoryl azide; triethylamine; In 1,4-dioxane; dichloromethane; 1: |Curtius Rearrangement;

Reference yield:

: 5043-14-1
7-bromonaphthalene-2-carboxylic acid

: 1613317-36-4
7-(4-phenylthiazol-2-yl)naphthalen-2-ylamine

Guidance literature:: Multi-step reaction with 6 steps

1: sulfuric acid / 18 h / Reflux; Inert atmosphere

2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / 3 h / 100 °C / Inert atmosphere

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate / 1,4-dioxane; water / 4 h / 100 °C / Inert atmosphere

4: lithium hydroxide; water / methanol; tetrahydrofuran / 18 h / 20 °C / Inert atmosphere

5: diphenyl phosphoryl azide; triethylamine / 1 h / 120 °C / Sealed tube; Microwave irradiation; Inert atmosphere

6: hydrogenchloride / dichloromethane; 1,4-dioxane / 6 h / 20 °C / Inert atmosphere

With hydrogenchloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sulfuric acid; diphenyl phosphoryl azide; water; potassium acetate; caesium carbonate; triethylamine; lithium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; 3: |Suzuki Coupling / 5: |Curtius Rearrangement;