2-cyclohexyl-N-[7-(4-phenylthiazol-2-yl)naphthalen-2-yl]succinamic acid

Base Information

Chemical Name:2-cyclohexyl-N-[7-(4-phenylthiazol-2-yl)naphthalen-2-yl]succinamic acid
CAS No.:1613317-20-6
Molecular Formula:C₂₉H₂₈N₂O₃S
Molecular Weight:484.619
Hs Code.:

Synonyms:2-cyclohexyl-N-[7-(4-phenylthiazol-2-yl)naphthalen-2-yl]succinamic acid

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Chemical Property of 2-cyclohexyl-N-[7-(4-phenylthiazol-2-yl)naphthalen-2-yl]succinamic acid

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Technology Process of 2-cyclohexyl-N-[7-(4-phenylthiazol-2-yl)naphthalen-2-yl]succinamic acid

There total 9 articles about 2-cyclohexyl-N-[7-(4-phenylthiazol-2-yl)naphthalen-2-yl]succinamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1613317-36-4
7-(4-phenylthiazol-2-yl)naphthalen-2-ylamine

: 5962-96-9
2-Cyclohexylbutandisaeure-anhydrid

: 1613317-20-6
2-cyclohexyl-N-[7-(4-phenylthiazol-2-yl)naphthalen-2-yl]succinamic acid

Guidance literature:: In chloroform; at 70 ℃; for 20h; Inert atmosphere;

Reference yield:

: 1613219-39-8
7-(4-phenylthiazol-2-yl)-naphthalene-2-carboxylic acid

: 1613317-20-6
2-cyclohexyl-N-[7-(4-phenylthiazol-2-yl)naphthalen-2-yl]succinamic acid

Guidance literature:: Multi-step reaction with 3 steps

1: diphenyl phosphoryl azide; triethylamine / 1 h / 120 °C / Sealed tube; Microwave irradiation; Inert atmosphere

2: hydrogenchloride / dichloromethane; 1,4-dioxane / 6 h / 20 °C / Inert atmosphere

3: chloroform / 20 h / 70 °C / Inert atmosphere

With hydrogenchloride; diphenyl phosphoryl azide; triethylamine; In 1,4-dioxane; dichloromethane; chloroform; 1: |Curtius Rearrangement;

Reference yield:

: 1613317-35-3
[7-(4-phenylthiazol-2-yl)naphthalen-2-yl]carbamic acid tert-butyl ester

: 1613317-20-6
2-cyclohexyl-N-[7-(4-phenylthiazol-2-yl)naphthalen-2-yl]succinamic acid

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / dichloromethane; 1,4-dioxane / 6 h / 20 °C / Inert atmosphere

2: chloroform / 20 h / 70 °C / Inert atmosphere

With hydrogenchloride; In 1,4-dioxane; dichloromethane; chloroform;