2-amino-2'-deuteriobiphenyl

Base Information

Chemical Name:2-amino-2'-deuteriobiphenyl
CAS No.:1283747-61-4
Molecular Formula:C₁₂H₁₁N
Molecular Weight:170.218
Hs Code.:

Synonyms:2-amino-2'-deuteriobiphenyl

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-amino-2'-deuteriobiphenyl

Chemical Property:

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Technology Process of 2-amino-2'-deuteriobiphenyl

There total 2 articles about 2-amino-2'-deuteriobiphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 4471-22-1
Phenyl-trityl-amine

: 88284-48-4
2-(trimethylsilyl)phenyl trifluoromethanesulfonate

: 1283747-61-4
2-amino-2'-deuteriobiphenyl

: 90-41-5
2-phenylaniline

Guidance literature:: Phenyl-trityl-amine; With tetrahydrofuran-d8; water-d2; sodium hydroxide; at 20 ℃; for 24h;

2-(trimethylsilyl)phenyl trifluoromethanesulfonate; With [D₃]acetonitrile; cesium fluoride; In toluene; Inert atmosphere; Sealed vial; Reflux;

With trifluoroacetic acid; at 20 ℃; for 0.333333h;
DOI:10.1002/anie.201106150

Reference yield:

: 62-53-3
aniline

: 1283747-61-4
2-amino-2'-deuteriobiphenyl

: 90-41-5
2-phenylaniline

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 20 °C

2.1: tetrahydrofuran-d8; water-d2; sodium hydroxide / 24 h / 20 °C

2.2: Inert atmosphere; Sealed vial; Reflux

2.3: 0.33 h / 20 °C

With tetrahydrofuran-d8; water-d2; triethylamine; sodium hydroxide; In dichloromethane;
DOI:10.1002/anie.201106150