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C15H19NO5

Base Information
  • Chemical Name:C15H19NO5
  • CAS No.:1430105-81-9
  • Molecular Formula:C15H19NO5
  • Molecular Weight:293.32
  • Hs Code.:
C<sub>15</sub>H<sub>19</sub>NO<sub>5</sub>

Synonyms:C15H19NO5

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Chemical Property of C15H19NO5
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Technology Process of C15H19NO5

There total 7 articles about C15H19NO5 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
cis-N-(benzyloxycarbonyl)-4-carboxy-L-proline methyl ester; With borane-THF; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;
With methanol; In tetrahydrofuran;
Guidance literature:
Multi-step reaction with 7 steps
1.1: thionyl chloride / Reflux
2.1: potassium carbonate / water; diethyl ether / 2 h / 0 - 20 °C
3.1: triethylamine / dichloromethane / 20 - 40 °C
4.1: cesium fluoride / N,N-dimethyl-formamide / 40 h / 60 °C
5.1: 1 h / 0 - 20 °C
5.2: 48 h / 20 °C
6.1: sodium hydroxide / tetrahydrofuran / 1.5 h / 0 - 20 °C
6.2: pH 3 - 4
7.1: borane-THF / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere
With thionyl chloride; borane-THF; potassium carbonate; triethylamine; cesium fluoride; sodium hydroxide; In tetrahydrofuran; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide;
Guidance literature:
Multi-step reaction with 6 steps
1.1: potassium carbonate / water; diethyl ether / 2 h / 0 - 20 °C
2.1: triethylamine / dichloromethane / 20 - 40 °C
3.1: cesium fluoride / N,N-dimethyl-formamide / 40 h / 60 °C
4.1: 1 h / 0 - 20 °C
4.2: 48 h / 20 °C
5.1: sodium hydroxide / tetrahydrofuran / 1.5 h / 0 - 20 °C
5.2: pH 3 - 4
6.1: borane-THF / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere
With borane-THF; potassium carbonate; triethylamine; cesium fluoride; sodium hydroxide; In tetrahydrofuran; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide;
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