1-(2S)-2-[(diisopropoxyphosphoryl)methoxy-3-(triphenylmethoxy)propyl-N⁴-docosanoyl-5-azacytosine]

Base Information

• Chemical Name: 1-(2S)-2-[(diisopropoxyphosphoryl)methoxy-3-(triphenylmethoxy)propyl-N⁴-docosanoyl-5-azacytosine]
• CAS No.: 1608457-43-7
• Molecular Formula: C₅₄H₈₁N₄O₇P
• Molecular Weight: 929.233

Synonyms:1-(2S)-2-[(diisopropoxyphosphoryl)methoxy-3-(triphenylmethoxy)propyl-N⁴-docosanoyl-5-azacytosine]

Chemical Property of 1-(2S)-2-[(diisopropoxyphosphoryl)methoxy-3-(triphenylmethoxy)propyl-N⁴-docosanoyl-5-azacytosine]

Chemical Property:

Purity/Quality:

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Technology Process of 1-(2S)-2-[(diisopropoxyphosphoryl)methoxy-3-(triphenylmethoxy)propyl-N⁴-docosanoyl-5-azacytosine]

There total 1 articles about 1-(2S)-2-[(diisopropoxyphosphoryl)methoxy-3-(triphenylmethoxy)propyl-N⁴-docosanoyl-5-azacytosine] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

1-{(2S)-2-[(diisopropoxyphosphoryl)methoxy-3-(triphenylmethoxy)]propyl}-5-azacytosine (933460-58-3) + docosanoyl chloride (21132-76-3) → 1-(2S)-2-[(diisopropoxyphosphoryl)methoxy-3-(triphenylmethoxy)propyl-N4-docosanoyl-5-azacytosine] (1608457-43-7)

Guidance literature:

In pyridine; at 20 ℃; for 48h;

DOI:10.1016/j.bmc.2014.03.031

Reference yield:

trimethylsilyl bromide (2857-97-8) + 1-(2S)-2-[(diisopropoxyphosphoryl)methoxy-3-(triphenylmethoxy)propyl-N4-docosanoyl-5-azacytosine] (1608457-43-7) → (S,E)-(8-amino-3-(hydroxymethyl)-6,10-dioxo-2-oxa-5,7,9-triazahentriacont-7-en-1-yl)phosphonic acid (1608459-53-5) + stearamide (124-26-5)

Guidance literature:

In acetonitrile; at 20 ℃; for 24h;

DOI:10.1016/j.bmc.2014.03.031

upstream raw materials:

1-{(2S)-2-[(diisopropoxyphosphoryl)methoxy-3-(triphenylmethoxy)]propyl}-5-azacytosine

docosanoyl chloride

Downstream raw materials:

(S,E)-(8-amino-3-(hydroxymethyl)-6,10-dioxo-2-oxa-5,7,9-triazahentriacont-7-en-1-yl)phosphonic acid

stearamide

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