diisopropyl 1-(4-bromobenzoyl)hydrazine-1,2-dicarboxylate

Base Information

Chemical Name:diisopropyl 1-(4-bromobenzoyl)hydrazine-1,2-dicarboxylate
CAS No.:1340546-31-7
Molecular Formula:C₁₅H₁₉BrN₂O₅
Molecular Weight:387.23
Hs Code.:

Synonyms:diisopropyl 1-(4-bromobenzoyl)hydrazine-1,2-dicarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diisopropyl 1-(4-bromobenzoyl)hydrazine-1,2-dicarboxylate

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Technology Process of diisopropyl 1-(4-bromobenzoyl)hydrazine-1,2-dicarboxylate

There total 1 articles about diisopropyl 1-(4-bromobenzoyl)hydrazine-1,2-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 2446-83-5
di-isopropyl azodicarboxylate

: 1122-91-4
4-bromo-benzaldehyde

: 1340546-31-7
diisopropyl 1-(4-bromobenzoyl)hydrazine-1,2-dicarboxylate

Guidance literature:: With pyridine; In N,N-dimethyl-formamide; at 140 ℃; for 0.166667h; Microwave irradiation; Sealed tube;
DOI:10.1016/j.tetlet.2014.11.090

Reference yield: 80.0%

: 1340546-31-7
diisopropyl 1-(4-bromobenzoyl)hydrazine-1,2-dicarboxylate

: C₁₁H₁₂BrNO₃

Guidance literature:: diisopropyl 1-(4-bromobenzoyl)hydrazine-1,2-dicarboxylate; With sodium hydride; In tetrahydrofuran; mineral oil;

With bromoacetic acid tert-butyl ester; In tetrahydrofuran; mineral oil; at 25 ℃; for 16h;
DOI:10.1039/c7ra04178k