tert-butyl 3-[benzyl(penta-3,4-dien-1-yl)carbamoyl]-2-oxopyrrolidine-1-carboxylate

Base Information

Chemical Name:tert-butyl 3-[benzyl(penta-3,4-dien-1-yl)carbamoyl]-2-oxopyrrolidine-1-carboxylate
CAS No.:1240791-69-8
Molecular Formula:C₂₂H₂₈N₂O₄
Molecular Weight:384.475
Hs Code.:

Synonyms:tert-butyl 3-[benzyl(penta-3,4-dien-1-yl)carbamoyl]-2-oxopyrrolidine-1-carboxylate

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Chemical Property of tert-butyl 3-[benzyl(penta-3,4-dien-1-yl)carbamoyl]-2-oxopyrrolidine-1-carboxylate

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Technology Process of tert-butyl 3-[benzyl(penta-3,4-dien-1-yl)carbamoyl]-2-oxopyrrolidine-1-carboxylate

There total 1 articles about tert-butyl 3-[benzyl(penta-3,4-dien-1-yl)carbamoyl]-2-oxopyrrolidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1240792-17-9
C₁₂H₁₅N

: 431079-79-7
1-(tert-butyl) 3-methyl 2-oxopyrrolidine-1,3-dicarboxylate

: 1240791-69-8
tert-butyl 3-[benzyl(penta-3,4-dien-1-yl)carbamoyl]-2-oxopyrrolidine-1-carboxylate

Guidance literature:: In toluene; Reflux;
DOI:10.1021/ol101425y

Reference yield: 74.0%

: 1240791-69-8
tert-butyl 3-[benzyl(penta-3,4-dien-1-yl)carbamoyl]-2-oxopyrrolidine-1-carboxylate

: 619-44-3
methyl 4-iodobenzoate

: (5R,10S)-tert-butyl 7-benzyl-10-{1-[4-(methoxycarbonyl)phenyl]vinyl}-1,6-dioxo-2,7-diazaspiro[4.5]decane-2-carboxylate

: C₃₀H₃₄N₂O₆

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium carbonate; 1,2-bis-(diphenylphosphino)ethane; In dimethyl sulfoxide; at 70 ℃; optical yield given as %de; diastereoselective reaction;
DOI:10.1021/ol101425y

Reference yield: 18.0%

: 1240791-69-8
tert-butyl 3-[benzyl(penta-3,4-dien-1-yl)carbamoyl]-2-oxopyrrolidine-1-carboxylate

: 1417504-14-3
1-iodo-9H-β-carboline

: tert-butyl (5R,10R)-7-benzyl-10-[1-(9H-β-carbolin-1-yl)vinyl]-1,6-dioxo-2,7-diazaspiro[4.5]decane-2-carboxylate

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium carbonate; 1,2-bis-(diphenylphosphino)ethane; In dimethyl sulfoxide; at 20 - 70 ℃; for 16h; stereoselective reaction; Inert atmosphere;
DOI:10.1016/j.tetlet.2012.10.111