(S)-5-{bis[3,5-bis(trifluoromethyl)phenyl](trimethylsiloxy)methyl}pyrrolidin-2-one

Base Information

Chemical Name:(S)-5-{bis[3,5-bis(trifluoromethyl)phenyl](trimethylsiloxy)methyl}pyrrolidin-2-one
CAS No.:1092807-28-7
Molecular Formula:C₂₄H₃₃NO₂Si
Molecular Weight:395.617
Hs Code.:

Synonyms:(S)-5-{bis[3,5-bis(trifluoromethyl)phenyl](trimethylsiloxy)methyl}pyrrolidin-2-one

Suppliers and Price of (S)-5-{bis[3,5-bis(trifluoromethyl)phenyl](trimethylsiloxy)methyl}pyrrolidin-2-one

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Chemical Property of (S)-5-{bis[3,5-bis(trifluoromethyl)phenyl](trimethylsiloxy)methyl}pyrrolidin-2-one

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Technology Process of (S)-5-{bis[3,5-bis(trifluoromethyl)phenyl](trimethylsiloxy)methyl}pyrrolidin-2-one

There total 1 articles about (S)-5-{bis[3,5-bis(trifluoromethyl)phenyl](trimethylsiloxy)methyl}pyrrolidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 27607-77-8
trimethylsilyl trifluoromethanesulfonate

: (S)-5-[bis(3,5-dimethylphenyl)(hydroxy)methyl]pyrrolidin-2-one

: 1092807-28-7
(S)-5-{bis[3,5-bis(trifluoromethyl)phenyl](trimethylsiloxy)methyl}pyrrolidin-2-one

Guidance literature:: With triethylamine; Inert atmosphere;
DOI:10.1055/s-2008-1067216

Reference yield: 82.0%

: 1092807-28-7
(S)-5-{bis[3,5-bis(trifluoromethyl)phenyl](trimethylsiloxy)methyl}pyrrolidin-2-one

: 420-37-1
trimethoxonium tetrafluoroborate

: 100-63-0
phenylhydrazine

: 1092807-27-6
(S)-5-[bis(3,5-dimethylphenyl)(trimethylsiloxy)methyl]-2-phenyl-6,7-dihydro-5H-pyrrolo[2,1-c]-1,2,4-triazol-2-ium tetrafluoroborate

Guidance literature:: (S)-5-{bis[3,5-bis(trifluoromethyl)phenyl](trimethylsiloxy)methyl}pyrrolidin-2-one; trimethoxonium tetrafluoroborate; Inert atmosphere;

phenylhydrazine; Inert atmosphere;

With trimethyl orthoformate; In methanol; at 90 ℃; for 4h; Inert atmosphere;
DOI:10.1055/s-2008-1067216