(S)-5-[bis(3,5-dimethylphenyl)(trimethylsiloxy)methyl]-2-phenyl-6,7-dihydro-5H-pyrrolo[2,1-c]-1,2,4-triazol-2-ium tetrafluoroborate

Base Information

Chemical Name:(S)-5-[bis(3,5-dimethylphenyl)(trimethylsiloxy)methyl]-2-phenyl-6,7-dihydro-5H-pyrrolo[2,1-c]-1,2,4-triazol-2-ium tetrafluoroborate
CAS No.:1092807-27-6
Molecular Formula:BF₄*C₃₁H₃₈N₃OSi
Molecular Weight:583.552
Hs Code.:

Synonyms:(S)-5-[bis(3,5-dimethylphenyl)(trimethylsiloxy)methyl]-2-phenyl-6,7-dihydro-5H-pyrrolo[2,1-c]-1,2,4-triazol-2-ium tetrafluoroborate

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Chemical Property of (S)-5-[bis(3,5-dimethylphenyl)(trimethylsiloxy)methyl]-2-phenyl-6,7-dihydro-5H-pyrrolo[2,1-c]-1,2,4-triazol-2-ium tetrafluoroborate

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Technology Process of (S)-5-[bis(3,5-dimethylphenyl)(trimethylsiloxy)methyl]-2-phenyl-6,7-dihydro-5H-pyrrolo[2,1-c]-1,2,4-triazol-2-ium tetrafluoroborate

There total 1 articles about (S)-5-[bis(3,5-dimethylphenyl)(trimethylsiloxy)methyl]-2-phenyl-6,7-dihydro-5H-pyrrolo[2,1-c]-1,2,4-triazol-2-ium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1092807-28-7
(S)-5-{bis[3,5-bis(trifluoromethyl)phenyl](trimethylsiloxy)methyl}pyrrolidin-2-one

: 420-37-1
trimethoxonium tetrafluoroborate

: 100-63-0
phenylhydrazine

: 1092807-27-6
(S)-5-[bis(3,5-dimethylphenyl)(trimethylsiloxy)methyl]-2-phenyl-6,7-dihydro-5H-pyrrolo[2,1-c]-1,2,4-triazol-2-ium tetrafluoroborate

Guidance literature:: (S)-5-{bis[3,5-bis(trifluoromethyl)phenyl](trimethylsiloxy)methyl}pyrrolidin-2-one; trimethoxonium tetrafluoroborate; Inert atmosphere;

phenylhydrazine; Inert atmosphere;

With trimethyl orthoformate; In methanol; at 90 ℃; for 4h; Inert atmosphere;
DOI:10.1055/s-2008-1067216