C₂₀H₃₄O₂Si

Base Information

Chemical Name:C₂₀H₃₄O₂Si
CAS No.:1454915-78-6
Molecular Formula:C₂₀H₃₄O₂Si
Molecular Weight:334.574
Hs Code.:

C<sub>20</sub>H<sub>34</sub>O<sub>2</sub>Si

Synonyms:C₂₀H₃₄O₂Si

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Chemical Property of C₂₀H₃₄O₂Si

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Technology Process of C₂₀H₃₄O₂Si

There total 7 articles about C₂₀H₃₄O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1454915-76-4
C₁₄H₂₀O₂

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1454915-78-6
C₂₀H₃₄O₂Si

Guidance literature:: With 1H-imidazole; In dichloromethane; at 0 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.1039/c3cc45170d

Reference yield:

: 1454915-73-1
ethyl 2-((1R,2S,6S)-2-hydroxy-3-methyl-6-(prop-1-en-2-yl)cyclohex-3-en-1-yl)acetate

: 1454915-78-6
C₂₀H₃₄O₂Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / toluene / 0.67 h / -78 °C / Inert atmosphere

2.2: sat. Na/K tartrate / 2 h / 20 °C / Inert atmosphere

3.1: tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

5.1: 1H-imidazole / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; triethylamine; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1039/c3cc45170d

Reference yield:

: 1454915-72-0
ethyl 2-((1R,6S)-3-methyl-2-oxo-6-(prop-1-en-2-yl)cyclohex-3-en-1-yl)acetate

: 1454915-78-6
C₂₀H₃₄O₂Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: cerium(III) chloride heptahydrate; sodium tetrahydroborate / methanol / -78 - -30 °C / Inert atmosphere

2.1: triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / toluene / 0.67 h / -78 °C / Inert atmosphere

3.2: sat. Na/K tartrate / 2 h / 20 °C / Inert atmosphere

4.1: tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

6.1: 1H-imidazole / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; sodium tetrahydroborate; cerium(III) chloride heptahydrate; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; triethylamine; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1039/c3cc45170d