(benzyloxycarbonyl)methyl di-tert-butyl phosphate

Base Information

Chemical Name:(benzyloxycarbonyl)methyl di-tert-butyl phosphate
CAS No.:130985-36-3
Molecular Formula:C₁₇H₂₇O₆P
Molecular Weight:358.372
Hs Code.:

Synonyms:(benzyloxycarbonyl)methyl di-tert-butyl phosphate

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Chemical Property of (benzyloxycarbonyl)methyl di-tert-butyl phosphate

Chemical Property:

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Technology Process of (benzyloxycarbonyl)methyl di-tert-butyl phosphate

There total 4 articles about (benzyloxycarbonyl)methyl di-tert-butyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 30379-58-9
benzyl glycolate

: 117924-33-1
di-tert-butyl N,N-diethylphosphoramidite

: 130985-36-3
(benzyloxycarbonyl)methyl di-tert-butyl phosphate

Guidance literature:: benzyl glycolate; di-tert-butyl N,N-diethylphosphoramidite; With 1H-tetrazole; In acetonitrile; at 20 ℃; for 2h;

With dihydrogen peroxide; In acetonitrile; at 0 ℃; for 1.5h;

Reference yield: 39.0%

: 139116-03-3
Benzyl 2-(Methanesulfonyl)acetate

: 68695-48-7
di-tert-butyl phosphoric acid tetra-n-butylammonium salt

: 130985-36-3
(benzyloxycarbonyl)methyl di-tert-butyl phosphate

Guidance literature:: In tetrahydrofuran;

Reference yield:

: 30379-58-9
benzyl glycolate

: 130985-36-3
(benzyloxycarbonyl)methyl di-tert-butyl phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-tetrazole / tetrahydrofuran / 2 h

2: m-chloroperbenzoic acid / CH₂Cl₂

With 1H-tetrazole; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm00106a026