(2R)-3-O-[α-D-galactopyranosyl-(1''''->6''')-O-β-D-galactopyranosyl]-sn-glycerol

Base Information

• Chemical Name: (2R)-3-O-[α-D-galactopyranosyl-(1''''->6''')-O-β-D-galactopyranosyl]-sn-glycerol
• CAS No.: 33600-42-9
• Molecular Formula: C₁₅H₂₈O₁₃
• Molecular Weight: 416.38

Synonyms:(2R)-3-O-[α-D-galactopyranosyl-(1''''->6''')-O-β-D-galactopyranosyl]-sn-glycerol

Chemical Property of (2R)-3-O-[α-D-galactopyranosyl-(1''''->6''')-O-β-D-galactopyranosyl]-sn-glycerol

Chemical Property:

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Technology Process of (2R)-3-O-[α-D-galactopyranosyl-(1''''->6''')-O-β-D-galactopyranosyl]-sn-glycerol

There total 5 articles about (2R)-3-O-[α-D-galactopyranosyl-(1''''->6''')-O-β-D-galactopyranosyl]-sn-glycerol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2S)-3-O-[α-D-galactopyranosyl-(1->6)-β-D-galactopyranosyl]-1-O-[(9Z,12Z,15Z)-octadeca-9,12,15-trienoyl]-sn-glycerol (145937-22-0) → (9Z,12Z,15Z)-octadeca-9-12,15-trienoic acid (463-40-1,1955-33-5,21661-10-9,21661-09-6,21661-13-2,21661-11-0) + methyl linolenate (301-00-8) + (2R)-3-O-[α-D-galactopyranosyl-(1''''->6''')-O-β-D-galactopyranosyl]-sn-glycerol (33600-42-9)

Guidance literature:

With potassium carbonate; Yield given. Yields of byproduct given;

DOI:10.1016/S0031-9422(00)80262-9

Reference yield:

methanol (67-56-1) + (2S)-1-O-octadecanoyl-2-O-tetradecanoyl-3-O-[α-D-galactopyranosyl-(1''->6')-O-β-D-galactopyranosyl]glycerol → methyl myristoate (124-10-7) + Methyl stearate (112-61-8) + (2R)-3-O-[α-D-galactopyranosyl-(1''''->6''')-O-β-D-galactopyranosyl]-sn-glycerol (33600-42-9)

Guidance literature:

With sodium methylate; at 20 ℃; for 3h;

DOI:10.1021/np0700164

Reference yield:

(2S)-1-O-(9Z,12Z)-octadecadienoyl-2-O-(7Z,10Z)-hexadecadienoyl-3-O-α-D-galactopyranosyl-(1->6)-β-D-galactopyranosyl-sn-glycerol → Methyl linoleate (112-63-0) + (7Z,10Z)-hexadecadienoic acid methyl ester (18829-90-8,16106-03-9) + (2R)-3-O-[α-D-galactopyranosyl-(1''''->6''')-O-β-D-galactopyranosyl]-sn-glycerol (33600-42-9)

Guidance literature:

With sodium methylate; In methanol; for 0.166667h; Ambient temperature;

DOI:10.1016/0031-9422(95)00458-J

upstream raw materials:

(2S)-3-O-[α-D-galactopyranosyl-(1->6)-β-D-galactopyranosyl]-1-O-[(9Z,12Z,15Z)-octadeca-9,12,15-trienoyl]-sn-glycerol

methanol

(6Z,9Z,12Z,15Z)-octadeca-6-9-12-15-tetraenoic acid (2R)-3-[(6-O-α-galactopyranosyl-β-D-galactopyranosyl)oxy]-2-hydroxypropyl ester

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