(1'RS,2'RS,3'SR,4'SR,6'RS)-N,N-dimethyl-1-<1-(2,2-dimethyl-1,1-diazanediyl)-2-(2',3'-dihydroxy-2',4'-dimethyl-6'-(phenylsulfonyl)cyclohexyl)ethyl>cyclopropanecarboxamide 2',3'-acetonide

Base Information

Chemical Name:(1'RS,2'RS,3'SR,4'SR,6'RS)-N,N-dimethyl-1-<1-(2,2-dimethyl-1,1-diazanediyl)-2-(2',3'-dihydroxy-2',4'-dimethyl-6'-(phenylsulfonyl)cyclohexyl)ethyl>cyclopropanecarboxamide 2',3'-acetonide
CAS No.:82769-90-2
Molecular Formula:C₂₇H₄₁N₃O₅S
Molecular Weight:519.706
Hs Code.:

(1'RS,2'RS,3'SR,4'SR,6'RS)-N,N-dimethyl-1-<1-(2,2-dimethyl-1,1-diazanediyl)-2-(2',3'-dihydroxy-2',4'-dimethyl-6'-(phenylsulfonyl)cyclohexyl)ethyl>cyclopropanecarboxamide 2',3'-acetonide

Synonyms:(1'RS,2'RS,3'SR,4'SR,6'RS)-N,N-dimethyl-1-<1-(2,2-dimethyl-1,1-diazanediyl)-2-(2',3'-dihydroxy-2',4'-dimethyl-6'-(phenylsulfonyl)cyclohexyl)ethyl>cyclopropanecarboxamide 2',3'-acetonide

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Chemical Property of (1'RS,2'RS,3'SR,4'SR,6'RS)-N,N-dimethyl-1-<1-(2,2-dimethyl-1,1-diazanediyl)-2-(2',3'-dihydroxy-2',4'-dimethyl-6'-(phenylsulfonyl)cyclohexyl)ethyl>cyclopropanecarboxamide 2',3'-acetonide

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Technology Process of (1'RS,2'RS,3'SR,4'SR,6'RS)-N,N-dimethyl-1-<1-(2,2-dimethyl-1,1-diazanediyl)-2-(2',3'-dihydroxy-2',4'-dimethyl-6'-(phenylsulfonyl)cyclohexyl)ethyl>cyclopropanecarboxamide 2',3'-acetonide

There total 5 articles about (1'RS,2'RS,3'SR,4'SR,6'RS)-N,N-dimethyl-1-<1-(2,2-dimethyl-1,1-diazanediyl)-2-(2',3'-dihydroxy-2',4'-dimethyl-6'-(phenylsulfonyl)cyclohexyl)ethyl>cyclopropanecarboxamide 2',3'-acetonide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.5%

: 82769-83-3
cis-3,4-dihydroxy-trans-3,5-dimethyl-1-(phenylsulfonyl)cyclohexene 3,4-acetonide

: 82769-89-9
anti-N,N-dimethyl-1-acetylcyclopropanecarboxamine dimethylhydrazone

: 82769-90-2
(1'RS,2'RS,3'SR,4'SR,6'RS)-N,N-dimethyl-1-<1-(2,2-dimethyl-1,1-diazanediyl)-2-(2',3'-dihydroxy-2',4'-dimethyl-6'-(phenylsulfonyl)cyclohexyl)ethyl>cyclopropanecarboxamide 2',3'-acetonide

Guidance literature:: With Diethoxy-methyl-(6-amino-hexylaminomethyl)-silan; In tetrahydrofuran; 1.) -78 deg C -> 0 deg C, 10 min, 2.) 0 deg C, 1 h;
DOI:10.1021/ja00385a030

Reference yield:

: 56172-71-5
1-Acetylcyclopropane-1-carboxylic acid

: 82769-90-2
(1'RS,2'RS,3'SR,4'SR,6'RS)-N,N-dimethyl-1-<1-(2,2-dimethyl-1,1-diazanediyl)-2-(2',3'-dihydroxy-2',4'-dimethyl-6'-(phenylsulfonyl)cyclohexyl)ethyl>cyclopropanecarboxamide 2',3'-acetonide

Guidance literature:: Multi-step reaction with 3 steps

1: 50 percent / benzene / 1 h / reflux -> room temperature

2: 77 percent / titanium tetrachloride, triethylamine / CH₂Cl₂ / 20 h / 25 °C

3: 89.5 percent / KDA / tetrahydrofuran / 1.) -78 deg C -> 0 deg C, 10 min, 2.) 0 deg C, 1 h

With Diethoxy-methyl-(6-amino-hexylaminomethyl)-silan; titanium tetrachloride; triethylamine; In tetrahydrofuran; dichloromethane; benzene;
DOI:10.1021/ja00385a030

Reference yield:

: 81939-86-8
trans,cis-3,5-dimethyl-1-phenylthio-trans,cis,cis-2,3,4-trihydroxycyclohexane 3,4-acetonide

: 82769-90-2
(1'RS,2'RS,3'SR,4'SR,6'RS)-N,N-dimethyl-1-<1-(2,2-dimethyl-1,1-diazanediyl)-2-(2',3'-dihydroxy-2',4'-dimethyl-6'-(phenylsulfonyl)cyclohexyl)ethyl>cyclopropanecarboxamide 2',3'-acetonide

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 1 h / Ambient temperature

2: 91 percent / phosphorus oxychloride / pyridine / 3 h / 110 °C

3: 89.5 percent / KDA / tetrahydrofuran / 1.) -78 deg C -> 0 deg C, 10 min, 2.) 0 deg C, 1 h

With Diethoxy-methyl-(6-amino-hexylaminomethyl)-silan; 3-chloro-benzenecarboperoxoic acid; trichlorophosphate; In tetrahydrofuran; pyridine; dichloromethane;
DOI:10.1021/ja00385a030