benzyl N-[4-(6-methoxypyridin-3-yl)phenyl]-N-(methylsulfonyl)homoserinate

Base Information

Chemical Name:benzyl N-[4-(6-methoxypyridin-3-yl)phenyl]-N-(methylsulfonyl)homoserinate
CAS No.:1369963-12-1
Molecular Formula:C₂₄H₂₆N₂O₆S
Molecular Weight:470.546
Hs Code.:

Synonyms:benzyl N-[4-(6-methoxypyridin-3-yl)phenyl]-N-(methylsulfonyl)homoserinate

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Chemical Property of benzyl N-[4-(6-methoxypyridin-3-yl)phenyl]-N-(methylsulfonyl)homoserinate

Chemical Property:

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Technology Process of benzyl N-[4-(6-methoxypyridin-3-yl)phenyl]-N-(methylsulfonyl)homoserinate

There total 7 articles about benzyl N-[4-(6-methoxypyridin-3-yl)phenyl]-N-(methylsulfonyl)homoserinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1369963-11-0
benzyl O-[tert-butyl(dimethyl)silyl]-N-[4-(6-methoxypyridin-3-yl)phenyl]-N-(methylsulfonyl)homoserinate

: 1369963-12-1
benzyl N-[4-(6-methoxypyridin-3-yl)phenyl]-N-(methylsulfonyl)homoserinate

Guidance literature:: benzyl O-[tert-butyl(dimethyl)silyl]-N-[4-(6-methoxypyridin-3-yl)phenyl]-N-(methylsulfonyl)homoserinate; With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 1h;

With water; In dichloromethane;

Reference yield:

: 106-40-1
4-bromo-aniline

: 1369963-12-1
benzyl N-[4-(6-methoxypyridin-3-yl)phenyl]-N-(methylsulfonyl)homoserinate

Guidance literature:: Multi-step reaction with 7 steps

1: pyridine / dichloromethane / 1 h

2: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0.5 h / 0 °C

3: sodium hydroxide / methanol / 1 h / 20 °C

4: N,N-dimethyl-formamide / 0 - 20 °C

5: 1H-imidazole / N,N-dimethyl-formamide / 1 h / 20 °C

6: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 3 h / 110 °C

7: boron trifluoride diethyl etherate / dichloromethane / 1 h / 20 °C

With pyridine; 1H-imidazole; di-isopropyl azodicarboxylate; boron trifluoride diethyl etherate; potassium carbonate; triphenylphosphine; sodium hydroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 4284-50-8
N-(4-bromophenyl)methanesulfonamide

: 1369963-12-1
benzyl N-[4-(6-methoxypyridin-3-yl)phenyl]-N-(methylsulfonyl)homoserinate

Guidance literature:: Multi-step reaction with 6 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0.5 h / 0 °C

2: sodium hydroxide / methanol / 1 h / 20 °C

3: N,N-dimethyl-formamide / 0 - 20 °C

4: 1H-imidazole / N,N-dimethyl-formamide / 1 h / 20 °C

5: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 3 h / 110 °C

6: boron trifluoride diethyl etherate / dichloromethane / 1 h / 20 °C

With 1H-imidazole; di-isopropyl azodicarboxylate; boron trifluoride diethyl etherate; potassium carbonate; triphenylphosphine; sodium hydroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;