benzyl N-(4-bromophenyl)-O-[tert-butyl(dimethyl)silyl]-N-(methylsulfonyl)homoserinate

Base Information

Chemical Name:benzyl N-(4-bromophenyl)-O-[tert-butyl(dimethyl)silyl]-N-(methylsulfonyl)homoserinate
CAS No.:1369963-10-9
Molecular Formula:C₂₄H₃₄BrNO₅SSi
Molecular Weight:556.593
Hs Code.:

Synonyms:benzyl N-(4-bromophenyl)-O-[tert-butyl(dimethyl)silyl]-N-(methylsulfonyl)homoserinate

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Chemical Property of benzyl N-(4-bromophenyl)-O-[tert-butyl(dimethyl)silyl]-N-(methylsulfonyl)homoserinate

Chemical Property:

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Technology Process of benzyl N-(4-bromophenyl)-O-[tert-butyl(dimethyl)silyl]-N-(methylsulfonyl)homoserinate

There total 5 articles about benzyl N-(4-bromophenyl)-O-[tert-butyl(dimethyl)silyl]-N-(methylsulfonyl)homoserinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1369963-09-6
benzyl N-(4-bromophenyl)-N-(methylsulfonyl)homoserinate

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1369963-10-9
benzyl N-(4-bromophenyl)-O-[tert-butyl(dimethyl)silyl]-N-(methylsulfonyl)homoserinate

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

Reference yield:

: 106-40-1
4-bromo-aniline

: 1369963-10-9
benzyl N-(4-bromophenyl)-O-[tert-butyl(dimethyl)silyl]-N-(methylsulfonyl)homoserinate

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / dichloromethane / 1 h

2: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0.5 h / 0 °C

3: sodium hydroxide / methanol / 1 h / 20 °C

4: N,N-dimethyl-formamide / 0 - 20 °C

5: 1H-imidazole / N,N-dimethyl-formamide / 1 h / 20 °C

With pyridine; 1H-imidazole; di-isopropyl azodicarboxylate; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 4284-50-8
N-(4-bromophenyl)methanesulfonamide

: 1369963-10-9
benzyl N-(4-bromophenyl)-O-[tert-butyl(dimethyl)silyl]-N-(methylsulfonyl)homoserinate

Guidance literature:: Multi-step reaction with 4 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0.5 h / 0 °C

2: sodium hydroxide / methanol / 1 h / 20 °C

3: N,N-dimethyl-formamide / 0 - 20 °C

4: 1H-imidazole / N,N-dimethyl-formamide / 1 h / 20 °C

With 1H-imidazole; di-isopropyl azodicarboxylate; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;