2,6-diacetylpyridine bis(N⁴-cyclohexylthiosemicarbazone)

Base Information

• Chemical Name: 2,6-diacetylpyridine bis(N⁴-cyclohexylthiosemicarbazone)
• CAS No.: 1217351-88-6
• Molecular Formula: C₂₃H₃₅N₇S₂
• Molecular Weight: 473.71
• Mol file: 1217351-88-6.mol

Synonyms:2,6-diacetylpyridine bis(N⁴-cyclohexylthiosemicarbazone)

Chemical Property of 2,6-diacetylpyridine bis(N⁴-cyclohexylthiosemicarbazone)

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 2,6-diacetylpyridine bis(N⁴-cyclohexylthiosemicarbazone)

There total 1 articles about 2,6-diacetylpyridine bis(N⁴-cyclohexylthiosemicarbazone) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

2,6-Diacetylpyridine (1129-30-2) + 4-cyclohexyl-thiosemicarbazide (21198-18-5) → 2,6-diacetylpyridine bis(N4-cyclohexylthiosemicarbazone) (1217351-88-6)

Guidance literature:

With acetic acid; In methanol; for 4h; Reflux;

DOI:10.1080/15533174.2013.867878

Reference yield: 79.0%

2,6-diacetylpyridine bis(N4-cyclohexylthiosemicarbazone) (1217351-88-6) + dimethyltin dichloride (753-73-1) → C25H39N7S2Sn

Guidance literature:

With sodium acetate; In methanol; for 1h; Reflux;

DOI:10.1080/15533174.2013.867878

Reference yield:

manganese(II) chloride tetrahydrate + 2,6-diacetylpyridine bis(N4-cyclohexylthiosemicarbazone) (1217351-88-6) → Mn(2,6-diacetylpyridine bis(4-cyclohexylthiosemicarbazone)Cl2*H2O

Guidance literature:

In methanol; chloroform; MnCl2*4H2O in MeOH refluxed with chloroform soln. of ligand; filtered, washed with MeOH and ether, dried in vacuo over P4O10; elem. anal.;

DOI:10.1016/j.saa.2009.11.022

upstream raw materials:

2,6-Diacetylpyridine

4-cyclohexyl-thiosemicarbazide