N-(N-phthaloyl-DL-alanyl)-N'-methyl-2'-benzoyl-4'-chlorosarcosinanilide

Base Information

Chemical Name:N-(N-phthaloyl-DL-alanyl)-N'-methyl-2'-benzoyl-4'-chlorosarcosinanilide
CAS No.:78823-14-0
Molecular Formula:C₂₈H₂₄ClN₃O₅
Molecular Weight:517.969
Hs Code.:

Synonyms:N-(N-phthaloyl-DL-alanyl)-N'-methyl-2'-benzoyl-4'-chlorosarcosinanilide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(N-phthaloyl-DL-alanyl)-N'-methyl-2'-benzoyl-4'-chlorosarcosinanilide

Chemical Property:

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Technology Process of N-(N-phthaloyl-DL-alanyl)-N'-methyl-2'-benzoyl-4'-chlorosarcosinanilide

There total 3 articles about N-(N-phthaloyl-DL-alanyl)-N'-methyl-2'-benzoyl-4'-chlorosarcosinanilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 57180-64-0
2-(methylamino-acetamido)-5-chloro-benzophenone

: 78823-14-0
N-(N-phthaloyl-DL-alanyl)-N'-methyl-2'-benzoyl-4'-chlorosarcosinanilide

Guidance literature:: Multi-step reaction with 2 steps

1: 1) SOCl₂ / 1) HMPA, MeCN, 15 min, 2) ether, -5 deg C - 0 deg C, 2 h

2: 1) NaH / 1) THF, 0 to -8 deg C, 30 min, 2) 0 - -8 deg C to RT, then 1.5 h

With thionyl chloride; sodium hydride;
DOI:10.1021/jo00335a034

Reference yield:

: 21860-84-4
2-phthalimidopropionic acid

: 78823-14-0
N-(N-phthaloyl-DL-alanyl)-N'-methyl-2'-benzoyl-4'-chlorosarcosinanilide

Guidance literature:: Multi-step reaction with 2 steps

1: 1) SOCl₂ / 1) HMPA, MeCN, 15 min, 2) ether, -5 deg C - 0 deg C, 2 h

2: 1) NaH / 1) THF, 0 to -8 deg C, 30 min, 2) 0 - -8 deg C to RT, then 1.5 h

With thionyl chloride; sodium hydride;
DOI:10.1021/jo00335a034

Reference yield:

: 78823-09-3
2'-Benzoyl-4'-chloro-N-(N-phthaloyl-DL-alanyl)sarcosinanilide

: 74-88-4
methyl iodide

: 78823-14-0
N-(N-phthaloyl-DL-alanyl)-N'-methyl-2'-benzoyl-4'-chlorosarcosinanilide

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1) THF, 0 to -8 deg C, 30 min, 2) 0 - -8 deg C to RT, then 1.5 h;
DOI:10.1021/jo00335a034