C₂₃H₂₉N₅O₃

Base Information

Chemical Name:C₂₃H₂₉N₅O₃
CAS No.:1246520-70-6
Molecular Formula:C₂₃H₂₉N₅O₃
Molecular Weight:423.515
Hs Code.:

C<sub>23</sub>H<sub>29</sub>N<sub>5</sub>O<sub>3</sub>

Synonyms:C₂₃H₂₉N₅O₃

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Chemical Property of C₂₃H₂₉N₅O₃

Chemical Property:

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Technology Process of C₂₃H₂₉N₅O₃

There total 12 articles about C₂₃H₂₉N₅O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1246521-42-5
C₁₉H₂₀N₄O₄

: 109-73-9,85404-21-3
N-butylamine

: 1246520-70-6
C₂₃H₂₉N₅O₃

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 16h; Cooling with ice;

Reference yield:

: 117007-52-0
3-iodo-1H-pyrazolo[3,4-b]pyridine

: 1246520-70-6
C₂₃H₂₉N₅O₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 3 h / Cooling with ice

1.2: 1 h / 20 °C / Cooling with ice

2.1: triethylamine / triphenylphosphine; palladium diacetate / 1,4-dioxane / 4 h / 100 °C / Inert atmosphere

3.1: sodium hydroxide; water / ethanol; tetrahydrofuran / 2 h / 20 °C / Cooling with ice

3.2: Cooling with ice

4.1: trifluoroacetic acid / 16 h / Reflux

5.1: hydrogen / palladium 10% on activated carbon / water; tetrahydrofuran; methanol / 3 h / 20 °C

6.1: N-chloro-succinimide; triphenylphosphine / tetrahydrofuran / 0.03 h / 20 °C

6.2: 18 h / 60 °C

7.1: sodium hydroxide; water / tetrahydrofuran; methanol / 18 h / 20 °C

8.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 16 h / 20 °C / Cooling with ice

With N-chloro-succinimide; water; hydrogen; sodium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; trifluoroacetic acid; sodium hydroxide; palladium 10% on activated carbon; palladium diacetate; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; water; N,N-dimethyl-formamide;

Reference yield:

: 36404-88-3
2-chloro-3-carbaldehydepyridine

: 1246520-70-6
C₂₃H₂₉N₅O₃

Guidance literature:: Multi-step reaction with 10 steps

1.1: toluene-4-sulfonic acid; hydrazine hydrate / 21 h / 120 °C / Cooling with ice

2.1: potassium hydroxide; iodine / N,N-dimethyl-formamide / 1 h / 20 °C / Cooling with ice

3.1: sodium hydride / N,N-dimethyl-formamide / 3 h / Cooling with ice

3.2: 1 h / 20 °C / Cooling with ice

4.1: triethylamine / triphenylphosphine; palladium diacetate / 1,4-dioxane / 4 h / 100 °C / Inert atmosphere

5.1: sodium hydroxide; water / ethanol; tetrahydrofuran / 2 h / 20 °C / Cooling with ice

5.2: Cooling with ice

6.1: trifluoroacetic acid / 16 h / Reflux

7.1: hydrogen / palladium 10% on activated carbon / water; tetrahydrofuran; methanol / 3 h / 20 °C

8.1: N-chloro-succinimide; triphenylphosphine / tetrahydrofuran / 0.03 h / 20 °C

8.2: 18 h / 60 °C

9.1: sodium hydroxide; water / tetrahydrofuran; methanol / 18 h / 20 °C

10.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 16 h / 20 °C / Cooling with ice

With N-chloro-succinimide; water; hydrogen; iodine; sodium hydride; benzotriazol-1-ol; toluene-4-sulfonic acid; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; trifluoroacetic acid; potassium hydroxide; sodium hydroxide; palladium 10% on activated carbon; palladium diacetate; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; water; N,N-dimethyl-formamide;