C₂₆H₂₃NO₅

Base Information

• Chemical Name: C₂₆H₂₃NO₅
• CAS No.: 1261079-23-5
• Molecular Formula: C₂₆H₂₃NO₅
• Molecular Weight: 429.472
• Mol file: 1261079-23-5.mol

Synonyms:C₂₆H₂₃NO₅

Chemical Property of C₂₆H₂₃NO₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₆H₂₃NO₅

There total 8 articles about C₂₆H₂₃NO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

1,3,4-tris(4-methoxyphenyl)-1H-pyrrole-2-carbaldehyde (1261079-22-4) → C26H23NO5 (1261079-23-5)

Guidance literature:

1,3,4-tris(4-methoxyphenyl)-1H-pyrrole-2-carbaldehyde; With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; water; In tetrahydrofuran; tert-butyl alcohol; at 10 ℃; for 24h;

With water; ammonium chloride; In tetrahydrofuran; tert-butyl alcohol;

DOI:10.1021/ol1027877

Reference yield:

1,3,4-tris(4-methoxyphenyl)-1H-pyrrole-2-carbaldehyde (1261079-22-4) → C26H23NO5 (1261079-23-5) + C26H22ClNO5

Guidance literature:

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; water; In tetrahydrofuran; tert-butyl alcohol; at 25 ℃;

DOI:10.1021/ol1027877

Reference yield:

4-Methoxyphenylacetaldehyde (5703-26-4) → C26H23NO5 (1261079-23-5)

Guidance literature:

Multi-step reaction with 3 steps

1.1: tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

1.2: 8 h / 60 °C / Inert atmosphere

2.1: trichlorophosphate / 0.17 h

2.2: 1 h / 60 °C

2.3: Cooling with ice; Heating

3.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene; water / tetrahydrofuran; tert-butyl alcohol / 24 h / 10 °C

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; water; trichlorophosphate; In tetrahydrofuran; tert-butyl alcohol; 2.2: Vilsmeier-Haack formylation / 3.1: Lindgren oxidation;

DOI:10.1021/ol1027877

upstream raw materials:

1,3,4-tris(4-methoxyphenyl)-1H-pyrrole

1,3,4-tris(4-methoxyphenyl)-1H-pyrrole-2-carbaldehyde

4-Methoxyphenylacetaldehyde

4-methoxy-aniline

Downstream raw materials:

1,3,4-tris(4-methoxyphenyl)-1H-pyrrole

2-methoxycarbonyl-3,4-di(4-methoxyphenyl)-N-4-methoxyphenylpyrrole