2S-(N,N'-bis-(t-butoxycarbonyl)hydrazino)-3-phenyl-1-propanoic acid, methyl ester

Base Information

Chemical Name:2S-(N,N'-bis-(t-butoxycarbonyl)hydrazino)-3-phenyl-1-propanoic acid, methyl ester
CAS No.:104267-06-3
Molecular Formula:C₂₀H₃₀N₂O₆
Molecular Weight:394.468
Hs Code.:

Synonyms:2S-(N,N'-bis-(t-butoxycarbonyl)hydrazino)-3-phenyl-1-propanoic acid, methyl ester

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Chemical Property of 2S-(N,N'-bis-(t-butoxycarbonyl)hydrazino)-3-phenyl-1-propanoic acid, methyl ester

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Technology Process of 2S-(N,N'-bis-(t-butoxycarbonyl)hydrazino)-3-phenyl-1-propanoic acid, methyl ester

There total 5 articles about 2S-(N,N'-bis-(t-butoxycarbonyl)hydrazino)-3-phenyl-1-propanoic acid, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: methoxymagnesium bromide

: 104266-94-6
(3(2S),4S)-3-(2-(N,N'-bis-(t-butoxycarbonyl)hydrazino)-3-phenyl-1-oxopropyl)-4-(phenylmethyl)-2-oxazolidinone

: 104267-06-3
2S-(N,N'-bis-(t-butoxycarbonyl)hydrazino)-3-phenyl-1-propanoic acid, methyl ester

Guidance literature:: In methanol; at 0 ℃; for 0.5h;
DOI:10.1021/ja00280a050

Reference yield: 89.0%

: 67-56-1
methanol

: 104266-94-6
(3(2S),4S)-3-(2-(N,N'-bis-(t-butoxycarbonyl)hydrazino)-3-phenyl-1-oxopropyl)-4-(phenylmethyl)-2-oxazolidinone

: 104267-06-3
2S-(N,N'-bis-(t-butoxycarbonyl)hydrazino)-3-phenyl-1-propanoic acid, methyl ester

Guidance literature:: With methylmagnesium bromide; In diethyl ether; at 0 ℃; for 0.5h;
DOI:10.1016/S0040-4020(01)86058-0

Reference yield:

: 870-50-8
di-tert-butyl-diazodicarboxylate

: 104267-06-3
2S-(N,N'-bis-(t-butoxycarbonyl)hydrazino)-3-phenyl-1-propanoic acid, methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: LDA / tetrahydrofuran; CH₂Cl₂; hexane / -78 °C

2: 89 percent / MeMgBr / diethyl ether / 0.5 h / 0 °C

With methylmagnesium bromide; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; hexane; dichloromethane;
DOI:10.1016/S0040-4020(01)86058-0