4-(N,N-dimethylamino)pyridinium 2-benzylthio-4-chloro-5-(1,3,4-oxadiazol-2-yl)-N-(pyridine-2-carbonyl)benzenesulfonamidate

Base Information

Chemical Name:4-(N,N-dimethylamino)pyridinium 2-benzylthio-4-chloro-5-(1,3,4-oxadiazol-2-yl)-N-(pyridine-2-carbonyl)benzenesulfonamidate
CAS No.:1380545-62-9
Molecular Formula:C₇H₁₀N₂*C₂₁H₁₅ClN₄O₄S₂
Molecular Weight:609.129
Hs Code.:

Synonyms:4-(N,N-dimethylamino)pyridinium 2-benzylthio-4-chloro-5-(1,3,4-oxadiazol-2-yl)-N-(pyridine-2-carbonyl)benzenesulfonamidate

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Chemical Property of 4-(N,N-dimethylamino)pyridinium 2-benzylthio-4-chloro-5-(1,3,4-oxadiazol-2-yl)-N-(pyridine-2-carbonyl)benzenesulfonamidate

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Technology Process of 4-(N,N-dimethylamino)pyridinium 2-benzylthio-4-chloro-5-(1,3,4-oxadiazol-2-yl)-N-(pyridine-2-carbonyl)benzenesulfonamidate

There total 3 articles about 4-(N,N-dimethylamino)pyridinium 2-benzylthio-4-chloro-5-(1,3,4-oxadiazol-2-yl)-N-(pyridine-2-carbonyl)benzenesulfonamidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 98-98-6
2-Picolinic acid

: 1122-58-3
dmap

: 1380545-54-9
2-benzylthio-4-chloro-5-(1,3,4-oxadiazol-2-yl)benzenesulfonamide

: 1380545-62-9
4-(N,N-dimethylamino)pyridinium 2-benzylthio-4-chloro-5-(1,3,4-oxadiazol-2-yl)-N-(pyridine-2-carbonyl)benzenesulfonamidate

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In acetonitrile; at 20 ℃;
DOI:10.1007/s00706-012-0732-6

Reference yield:

: 18648-15-2
2,4-dichloro-5-(carbazoyl)benzenesulfonamide

: 1380545-62-9
4-(N,N-dimethylamino)pyridinium 2-benzylthio-4-chloro-5-(1,3,4-oxadiazol-2-yl)-N-(pyridine-2-carbonyl)benzenesulfonamidate

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / Reflux

2: tetrabutylammomium bromide; potassium carbonate / water; acetonitrile / 24 h / 25 °C / Inert atmosphere

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / acetonitrile / 20 °C

With tetrabutylammomium bromide; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In water; acetic acid; acetonitrile;
DOI:10.1007/s00706-012-0732-6

Reference yield:

: 1380545-52-7
2,4-dichloro-5-(1,3,4-oxadiazol-2-yl)benzenesulfonamide

: 1380545-62-9
4-(N,N-dimethylamino)pyridinium 2-benzylthio-4-chloro-5-(1,3,4-oxadiazol-2-yl)-N-(pyridine-2-carbonyl)benzenesulfonamidate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutylammomium bromide; potassium carbonate / water; acetonitrile / 24 h / 25 °C / Inert atmosphere

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / acetonitrile / 20 °C

With tetrabutylammomium bromide; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In water; acetonitrile;
DOI:10.1007/s00706-012-0732-6