1-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cyclohexan-cis-1,4-diyl diacetate

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Chemical Name:1-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cyclohexan-cis-1,4-diyl diacetate
CAS No.:1224949-99-8
Molecular Formula:C₂₇H₃₀N₂O₅
Molecular Weight:462.546
Hs Code.:

Synonyms:1-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cyclohexan-cis-1,4-diyl diacetate

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Chemical Property of 1-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cyclohexan-cis-1,4-diyl diacetate

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Technology Process of 1-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cyclohexan-cis-1,4-diyl diacetate

There total 7 articles about 1-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cyclohexan-cis-1,4-diyl diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1224949-51-2
8-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-1,4-dioxaspiro[4.5]decan-8-ol

: 1224949-99-8
1-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cyclohexan-cis-1,4-diyl diacetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride; water / tetrahydrofuran / 15 h / 20 °C

1.2: 0 °C

2.1: sodium tetrahydroborate; methanol / 2 h / 20 °C

3.1: dmap; pyridine / dichloromethane / 66 h / 20 °C

With pyridine; hydrogenchloride; methanol; dmap; sodium tetrahydroborate; water; In tetrahydrofuran; dichloromethane;

Reference yield:

: 1224949-36-3
3-(8-hydroxy-1,4-dioxaspiro[4.5]decan-8-yl)-1-(p-tolyl)-2-propyn-1-one

: 1224949-99-8
1-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cyclohexan-cis-1,4-diyl diacetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / ethanol / 0.5 h / 20 °C

1.2: 15 h / 20 °C

2.1: hydrogenchloride; water / tetrahydrofuran / 15 h / 20 °C

2.2: 0 °C

3.1: sodium tetrahydroborate; methanol / 2 h / 20 °C

4.1: dmap; pyridine / dichloromethane / 66 h / 20 °C

With pyridine; hydrogenchloride; methanol; dmap; sodium tetrahydroborate; water; triethylamine; In tetrahydrofuran; ethanol; dichloromethane;

Reference yield:

: 4746-97-8
cyclohexanedione monoethylene ketal

: 1224949-99-8
1-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cyclohexan-cis-1,4-diyl diacetate

Guidance literature:: Multi-step reaction with 8 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -76 °C

1.2: 2 h / -74 °C

2.1: potassium carbonate; methanol / 2 h / 20 °C

3.1: n-butyllithium / hexane; tetrahydrofuran / 0.92 h / -72 °C

3.2: 0.58 h / -72 °C

4.1: manganese(IV) oxide / dichloromethane / 15 h / 20 °C

5.1: triethylamine / ethanol / 0.5 h / 20 °C

5.2: 15 h / 20 °C

6.1: hydrogenchloride; water / tetrahydrofuran / 15 h / 20 °C

6.2: 0 °C

7.1: sodium tetrahydroborate; methanol / 2 h / 20 °C

8.1: dmap; pyridine / dichloromethane / 66 h / 20 °C

With pyridine; hydrogenchloride; methanol; dmap; manganese(IV) oxide; sodium tetrahydroborate; n-butyllithium; water; potassium carbonate; triethylamine; In tetrahydrofuran; ethanol; hexane; dichloromethane;