1,2-O-isopropylidene-3-O-(13-phenyl-3,6,9,12-tetraoxatridecyl)-sn-glycerol

Base Information

Chemical Name:1,2-O-isopropylidene-3-O-(13-phenyl-3,6,9,12-tetraoxatridecyl)-sn-glycerol
CAS No.:1616876-38-0
Molecular Formula:C₂₁H₃₄O₇
Molecular Weight:398.497
Hs Code.:

Synonyms:1,2-O-isopropylidene-3-O-(13-phenyl-3,6,9,12-tetraoxatridecyl)-sn-glycerol

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Chemical Property of 1,2-O-isopropylidene-3-O-(13-phenyl-3,6,9,12-tetraoxatridecyl)-sn-glycerol

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Technology Process of 1,2-O-isopropylidene-3-O-(13-phenyl-3,6,9,12-tetraoxatridecyl)-sn-glycerol

There total 4 articles about 1,2-O-isopropylidene-3-O-(13-phenyl-3,6,9,12-tetraoxatridecyl)-sn-glycerol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 477781-69-4
1-phenyl-2,5,8,11-tetraoxatridecan-13-yl methanesulfonate

: 22323-82-6,36543-79-0
(S)-(+)-(2,2-dimethyl-[1,3]dioxolan-4-yl)methanol

: 1616876-38-0
1,2-O-isopropylidene-3-O-(13-phenyl-3,6,9,12-tetraoxatridecyl)-sn-glycerol

Guidance literature:: With potassium hydroxide; In dimethyl sulfoxide; at 20 - 40 ℃; for 21h; Inert atmosphere;
DOI:10.1039/c4cc00863d

Reference yield:

: 86259-87-2,1201808-31-2
1-phenyl-2,5,8,11-tetraoxatridecan-13-ol

: 1616876-38-0
1,2-O-isopropylidene-3-O-(13-phenyl-3,6,9,12-tetraoxatridecyl)-sn-glycerol

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 15.16 h / -30 - 20 °C

2: potassium hydroxide / dimethyl sulfoxide / 21 h / 20 - 40 °C / Inert atmosphere

With triethylamine; potassium hydroxide; In dichloromethane; dimethyl sulfoxide;
DOI:10.1039/c4cc00863d

Reference yield:

: 112-60-7
Tetraethylene glycol

: 1616876-38-0
1,2-O-isopropylidene-3-O-(13-phenyl-3,6,9,12-tetraoxatridecyl)-sn-glycerol

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 - 20 °C / Inert atmosphere

1.2: 20 h / 20 °C / Inert atmosphere

2.1: triethylamine / dichloromethane / 15.16 h / -30 - 20 °C

3.1: potassium hydroxide / dimethyl sulfoxide / 21 h / 20 - 40 °C / Inert atmosphere

With sodium hydride; triethylamine; potassium hydroxide; In dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; mineral oil;
DOI:10.1039/c4cc00863d