Technology Process of 4-acetyl-2-methyl benzoyl chloride
There total 4 articles about 4-acetyl-2-methyl benzoyl chloride which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
oxalyl dichloride;
N,N-dimethyl-formamide;
In
dichloromethane;
at 20 ℃;
for 3h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: aluminum (III) chloride / dichloromethane / 26 h / 20 °C / Reflux
2: dimethyl sulfoxide / 12 h / 120 °C
3: water; sulfuric acid; acetic acid / 20 °C / Reflux
4: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 20 °C
With
aluminum (III) chloride; oxalyl dichloride; sulfuric acid; water; acetic acid;
N,N-dimethyl-formamide;
In
dichloromethane; dimethyl sulfoxide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dimethyl sulfoxide / 12 h / 120 °C
2: water; sulfuric acid; acetic acid / 20 °C / Reflux
3: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 20 °C
With
oxalyl dichloride; sulfuric acid; water; acetic acid;
N,N-dimethyl-formamide;
In
dichloromethane; dimethyl sulfoxide;
