C₄₁H₄₇N₃O₁₃

Base Information

Chemical Name:C₄₁H₄₇N₃O₁₃
CAS No.:1338925-57-7
Molecular Formula:C₄₁H₄₇N₃O₁₃
Molecular Weight:789.836
Hs Code.:

C<sub>41</sub>H<sub>47</sub>N<sub>3</sub>O<sub>13</sub>

Synonyms:C₄₁H₄₇N₃O₁₃

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Chemical Property of C₄₁H₄₇N₃O₁₃

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Technology Process of C₄₁H₄₇N₃O₁₃

There total 13 articles about C₄₁H₄₇N₃O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1338925-52-2
C₃₄H₃₉N₃O₈

: 122089-71-8
2,3,4-tri-O-acetyl-L-rhamnopyranosyl trichloroacetimidate

: 1338925-57-7
C₄₁H₄₇N₃O₁₃

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at -78 - 20 ℃; Molecular sieve;
DOI:10.1021/ja207318n

Reference yield:

: 1086703-05-0
(S)-2-(tert-butoxycarbonyl(methyl)amino)-2-(4-hydroxy-3-iodophenyl)acetic acid

: 1338925-57-7
C₄₁H₄₇N₃O₁₃

Guidance literature:: Multi-step reaction with 5 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 0 - 20 °C

2: trimethyltin(IV) hydroxide / 1,2-dichloro-ethane / 4 h / 20 - 75 °C / Inert atmosphere

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide; acetonitrile / 0 - 20 °C

4: bis(tri-t-butylphosphine)palladium⁽⁰⁾; potassium carbonate / dimethyl sulfoxide / 24 h / 90 °C / Inert atmosphere

5: boron trifluoride diethyl etherate / dichloromethane / -78 - 20 °C / Molecular sieve

With bis(tri-t-butylphosphine)palladium⁽⁰⁾; boron trifluoride diethyl etherate; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trimethyltin(IV) hydroxide; In dichloromethane; dimethyl sulfoxide; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja207318n

Reference yield:

: 1086703-03-8
(S)-2-(tert-butoxycarbonyl(methyl)amino)-2-(4-hydroxy-3-iodophenyl)acetic acid

: 1338925-57-7
C₄₁H₄₇N₃O₁₃

Guidance literature:: Multi-step reaction with 7 steps

1: triethylsilane; trifluoroacetic acid / 24 h / 0 - 20 °C

2: sodium hydrogencarbonate; sodium hydroxide / tetrahydrofuran; water / 8 h / 0 - 20 °C / pH 7

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 0 - 20 °C

4: trimethyltin(IV) hydroxide / 1,2-dichloro-ethane / 4 h / 20 - 75 °C / Inert atmosphere

5: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide; acetonitrile / 0 - 20 °C

6: bis(tri-t-butylphosphine)palladium⁽⁰⁾; potassium carbonate / dimethyl sulfoxide / 24 h / 90 °C / Inert atmosphere

7: boron trifluoride diethyl etherate / dichloromethane / -78 - 20 °C / Molecular sieve

With triethylsilane; bis(tri-t-butylphosphine)palladium⁽⁰⁾; boron trifluoride diethyl etherate; sodium hydrogencarbonate; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trimethyltin(IV) hydroxide; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja207318n