2-(4-tert-butylcyclohexylidene)ethyl picolinate

Base Information

Chemical Name:2-(4-tert-butylcyclohexylidene)ethyl picolinate
CAS No.:1240401-57-3
Molecular Formula:C₁₈H₂₅NO₂
Molecular Weight:287.402
Hs Code.:

Synonyms:2-(4-tert-butylcyclohexylidene)ethyl picolinate

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Chemical Property of 2-(4-tert-butylcyclohexylidene)ethyl picolinate

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Technology Process of 2-(4-tert-butylcyclohexylidene)ethyl picolinate

There total 1 articles about 2-(4-tert-butylcyclohexylidene)ethyl picolinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-98-6
2-Picolinic acid

: 41498-18-4,85048-19-7,145549-19-5
2-(4-(tert-butyl)cyclohexylidene)ethanol

: 1240401-57-3
2-(4-tert-butylcyclohexylidene)ethyl picolinate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; Cooling with ice;
DOI:10.1039/c0cc00653j

Reference yield: 94.0%

: 693-03-8
n-butyl magnesium bromide

: 1240401-57-3
2-(4-tert-butylcyclohexylidene)ethyl picolinate

: 1240401-75-5
4-tert-butyl-1-butyl-1-vinylcyclohexane

Guidance literature:: n-butyl magnesium bromide; With copper(I) bromide dimethylsulfide complex; zinc(II) iodide; In tetrahydrofuran; at 0 ℃; for 0.5h;

2-(4-tert-butylcyclohexylidene)ethyl picolinate; In tetrahydrofuran; at -40 - -10 ℃; for 1h; stereoselective reaction;
DOI:10.1039/c0cc00653j

Reference yield: 94.0%

: 1240401-57-3
2-(4-tert-butylcyclohexylidene)ethyl picolinate

: 75-16-1
methylmagnesium bromide

: 41498-78-6
(1s,4s)-4-tert-butyl-1-methyl-1-vinylcyclohexane

Guidance literature:: methylmagnesium bromide; With copper(I) bromide dimethylsulfide complex; zinc dibromide; In tetrahydrofuran; at 0 ℃; for 0.5h;

2-(4-tert-butylcyclohexylidene)ethyl picolinate; In tetrahydrofuran; at -40 - -10 ℃; for 1h; optical yield given as %de; stereoselective reaction;
DOI:10.1039/c0cc00653j