2,4-dinitro-benzoic acid p-toluidide

Base Information

• Chemical Name: 2,4-dinitro-benzoic acid p-toluidide
• CAS No.: 374632-10-7
• Molecular Formula: C₁₄H₁₁N₃O₅
• Molecular Weight: 301.258
• Mol file: 374632-10-7.mol

Synonyms:2,4-dinitro-benzoic acid p-toluidide

Chemical Property of 2,4-dinitro-benzoic acid p-toluidide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 2,4-dinitro-benzoic acid p-toluidide

There total 4 articles about 2,4-dinitro-benzoic acid p-toluidide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,4-dinitrobenzoyl chloride (20195-22-6) + p-toluidine (106-49-0,12221-03-3) → 2,4-dinitro-benzoic acid p-toluidide (374632-10-7)

Guidance literature:

Reference yield:

2,4-dinitrobenzoic acid (610-30-0) → 2,4-dinitro-benzoic acid p-toluidide (374632-10-7)

Guidance literature:

Multi-step reaction with 2 steps

1: SOCl₂ / dimethylformamide / 3 h / Heating

2: aq. NaHCO₃ / benzene / 5 °C

With thionyl chloride; sodium hydrogencarbonate; In N,N-dimethyl-formamide; benzene;

DOI:10.1055/s-2001-16764

Reference yield:

1-methyl-4-nitrosobenzene (623-11-0) + 2,4-dinitrotoluene (121-14-2) → 2,4-dinitro-benzaldehyde-(N-p-tolyl oxime ) + 2,4-dinitro-benzoic acid p-toluidide (374632-10-7)

Guidance literature:

With ethanol; sodium carbonate;

upstream raw materials:

1-methyl-4-nitrosobenzene

2,4-dinitrotoluene

2,4-dinitrobenzoyl chloride

p-toluidine

Downstream raw materials:

2-benzylsulfanyl-4-nitro-N-p-tolyl-benzamide

Refernces