2,2,2',2'-Tetramethyl-N,N'-(3,4,5,6-tetramethylphen-1,2-ylen)bis

Base Information

Chemical Name:2,2,2',2'-Tetramethyl-N,N'-(3,4,5,6-tetramethylphen-1,2-ylen)bis
CAS No.:147503-27-3
Molecular Formula:C₂₀H₃₂N₂O₂
Molecular Weight:332.486
Hs Code.:

2,2,2',2'-Tetramethyl-N,N'-(3,4,5,6-tetramethylphen-1,2-ylen)bis<propanamid>

Synonyms:2,2,2',2'-Tetramethyl-N,N'-(3,4,5,6-tetramethylphen-1,2-ylen)bis

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2,2',2'-Tetramethyl-N,N'-(3,4,5,6-tetramethylphen-1,2-ylen)bis

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Technology Process of 2,2,2',2'-Tetramethyl-N,N'-(3,4,5,6-tetramethylphen-1,2-ylen)bis

There total 3 articles about 2,2,2',2'-Tetramethyl-N,N'-(3,4,5,6-tetramethylphen-1,2-ylen)bis which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 67130-14-7
1,2-diamino-3,4,5,6-tetramethylbenzene

: 3282-30-2
pivaloyl chloride

: 147503-27-3
2,2,2',2'-Tetramethyl-N,N'-(3,4,5,6-tetramethylphen-1,2-ylen)bis

Guidance literature:: With triethylamine; In dichloromethane; Ambient temperature;
DOI:10.1002/hlca.19930760120

Reference yield:

: 488-23-3
1,2,3,4-Tetramethylbenzene

: 147503-27-3
2,2,2',2'-Tetramethyl-N,N'-(3,4,5,6-tetramethylphen-1,2-ylen)bis

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / HNO₃, H₂SO₄ / CHCl₃ / 0 °C

2: 91 percent / H₂ / 5percent Pd-C / ethanol / Ambient temperature

3: 96 percent / NEt₃ / CH₂Cl₂ / Ambient temperature

With sulfuric acid; hydrogen; nitric acid; triethylamine; palladium on activated charcoal; In ethanol; dichloromethane; chloroform;
DOI:10.1002/hlca.19930760120

Reference yield:

: 18801-63-3
3,4,5,6-tetramethyl-1,2-dinitrobenzene

: 147503-27-3
2,2,2',2'-Tetramethyl-N,N'-(3,4,5,6-tetramethylphen-1,2-ylen)bis

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / H₂ / 5percent Pd-C / ethanol / Ambient temperature

2: 96 percent / NEt₃ / CH₂Cl₂ / Ambient temperature

With hydrogen; triethylamine; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1002/hlca.19930760120